Organometallics

, том 31 , издание 24 , страницы 8627-8638

Complexes of Donor–Acceptor Cyclopropanes with Tin, Titanium, and Gallium Chlorides — Mechanism Studies

Тип публикации: Journal Article

Дата публикации: 2012-12-11

American Chemical Society (ACS)

Organometallics

scimago Q2

wos Q1

БС1

SJR: 0.676

CiteScore: 5.1

Impact factor: 2.9

ISSN: 02767333, 15206041

DOI: 10.1021/om301072v

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Organic Chemistry

Inorganic Chemistry

Physical and Theoretical Chemistry

Краткое описание

Hitherto unknown complexes of dimethyl cyclopropane-1,1-dicarboxylate with Lewis acids (Sn, Ti, and Ga chlorides) have been isolated and characterized. Their structures, which were previously assumed from theoretical considerations, have been confirmed, and the activating effect of Lewis acids on the cyclopropane ring has been shown experimentally. A single crystal of the complex with SnCl4 has been obtained, and an X-ray diffraction study has been performed. Hitherto unknown complexes of donor–acceptor cyclopropanes with GaCl3 belonging to a new type and having a 1,2-dipole (ylide) structure have been obtained and characterized. 1D and 2D NMR spectroscopy on 1H, 13C, 35Cl, 71Ga, and 119Sn nuclei were used to study the structures of the complexes. Furthermore, DOSY diffusion NMR spectroscopy was used to determine the diffusion coefficient in solution and the molecular masses of the complexes. The data obtained enrich the picture of transformations of donor–acceptor cyclopropanes widely used in organic syn...

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Novikov R. G. et al. Complexes of Donor–Acceptor Cyclopropanes with Tin, Titanium, and Gallium Chlorides — Mechanism Studies // Organometallics. 2012. Vol. 31. No. 24. pp. 8627-8638.

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Novikov R. G., Balakirev D. O., Timofeev V. P., Tomilov Y. V. Complexes of Donor–Acceptor Cyclopropanes with Tin, Titanium, and Gallium Chlorides — Mechanism Studies // Organometallics. 2012. Vol. 31. No. 24. pp. 8627-8638.

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TY - JOUR

DO - 10.1021/om301072v

UR - https://doi.org/10.1021/om301072v

TI - Complexes of Donor–Acceptor Cyclopropanes with Tin, Titanium, and Gallium Chlorides — Mechanism Studies

T2 - Organometallics

AU - Novikov, Roman G.

AU - Balakirev, Dmitry O.

AU - Timofeev, Vladimir P

AU - Tomilov, Yury V.

PY - 2012

DA - 2012/12/11

PB - American Chemical Society (ACS)

SP - 8627-8638

IS - 24

VL - 31

SN - 0276-7333

SN - 1520-6041

ER -

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@article{2012_Novikov,

author = {Roman G. Novikov and Dmitry O. Balakirev and Vladimir P Timofeev and Yury V. Tomilov},

title = {Complexes of Donor–Acceptor Cyclopropanes with Tin, Titanium, and Gallium Chlorides — Mechanism Studies},

journal = {Organometallics},

year = {2012},

volume = {31},

publisher = {American Chemical Society (ACS)},

month = {dec},

url = {https://doi.org/10.1021/om301072v},

number = {24},

pages = {8627--8638},

doi = {10.1021/om301072v}

}

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Novikov, Roman G., et al. “Complexes of Donor–Acceptor Cyclopropanes with Tin, Titanium, and Gallium Chlorides — Mechanism Studies.” Organometallics, vol. 31, no. 24, Dec. 2012, pp. 8627-8638. https://doi.org/10.1021/om301072v.