Ring-Methyl Activation in Pentamethylcyclopentadienyl Complexes. 5.1 Syntheses and Structures of Tetramethylfulvene Complexes of Ruthenium(II)
Тип публикации: Journal Article
Дата публикации: 1996-01-09
scimago Q2
wos Q1
БС1
SJR: 0.676
CiteScore: 5.1
Impact factor: 2.9
ISSN: 02767333, 15206041
Organic Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
As previously reported, [{(η5-C5Me5)RuCl2}2], 1a, is oxygenated to the μ-oxo complex, [{(η5-C5Me5)RuCl2}2O], 2a (Angelici, R. J.; et al Organometallics 1992, 11, 2303). It is now shown that 2a spontaneously decomposes in chloroform solution by activation of a methyl C−H bond, to give the dinuclear tetramethylfulvene (TMF) complex [{(η6-C5Me4CH2)RuCl2}2], 3a, and water. The structure of 3a in the solid state (established by an X-ray structure determination) showed two crystallographically different but structurally similar centrosymmetric dinuclear molecules, each having a TMF η6-bonded to ruthenium(II). Each metal atom is approximately octahedrally coordinated by the η6-C5Me4CH2 and by three chlorides, two of which bridge to the other ruthenium and one of which is terminal. The chloride bridges are broken on reaction with ligands L to give [(η6-C5Me4CH2)RuCl2(L)], 4a (L = py), or 5a (L = Me2SO). All the complexes 2−5 are diamagnetic. NMR spectra of solutions of 3a show the presence of several structural i...
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Fan L. et al. Ring-Methyl Activation in Pentamethylcyclopentadienyl Complexes. 5.1 Syntheses and Structures of Tetramethylfulvene Complexes of Ruthenium(II) // Organometallics. 1996. Vol. 15. No. 1. pp. 98-104.
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Fan L., Wei C., Aigbirhio F. I., Turner M., Gusev O. V., Morozova L. N., Knowles D. R. T., Maitlis P. M. Ring-Methyl Activation in Pentamethylcyclopentadienyl Complexes. 5.1 Syntheses and Structures of Tetramethylfulvene Complexes of Ruthenium(II) // Organometallics. 1996. Vol. 15. No. 1. pp. 98-104.
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TY - JOUR
DO - 10.1021/om950462z
UR - https://doi.org/10.1021/om950462z
TI - Ring-Methyl Activation in Pentamethylcyclopentadienyl Complexes. 5.1 Syntheses and Structures of Tetramethylfulvene Complexes of Ruthenium(II)
T2 - Organometallics
AU - Fan, Li
AU - Wei, Chunghong
AU - Aigbirhio, Franklin I.
AU - Turner, Michael
AU - Gusev, Oleg V
AU - Morozova, Larissa N
AU - Knowles, Daniel R T
AU - Maitlis, Peter M.
PY - 1996
DA - 1996/01/09
PB - American Chemical Society (ACS)
SP - 98-104
IS - 1
VL - 15
SN - 0276-7333
SN - 1520-6041
ER -
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@article{1996_Fan,
author = {Li Fan and Chunghong Wei and Franklin I. Aigbirhio and Michael Turner and Oleg V Gusev and Larissa N Morozova and Daniel R T Knowles and Peter M. Maitlis},
title = {Ring-Methyl Activation in Pentamethylcyclopentadienyl Complexes. 5.1 Syntheses and Structures of Tetramethylfulvene Complexes of Ruthenium(II)},
journal = {Organometallics},
year = {1996},
volume = {15},
publisher = {American Chemical Society (ACS)},
month = {jan},
url = {https://doi.org/10.1021/om950462z},
number = {1},
pages = {98--104},
doi = {10.1021/om950462z}
}
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MLA
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Fan, Li, et al. “Ring-Methyl Activation in Pentamethylcyclopentadienyl Complexes. 5.1 Syntheses and Structures of Tetramethylfulvene Complexes of Ruthenium(II).” Organometallics, vol. 15, no. 1, Jan. 1996, pp. 98-104. https://doi.org/10.1021/om950462z.