Open Access

Nature Communications, volume 9, issue 1, publication number 1269

Synthesis of AgN5 and its extended 3D energetic framework

Chengguo Sun ^{1, 2}

Chong Zhang ¹

Chao Jiang ¹

Chen Yang ¹

Yang Du ¹

Yue Zhao ¹

Bingcheng Hu ¹

Zhansheng Zheng ¹

Karl O. Christe ^{1, 3}

Hide authors affiliations Show authors affiliations: 3 affiliations

School of Chemical Engineering, Nanjing University of Science and Technology, Nanjing, China |

School of Chemical Engineering, University of Science and Technology LiaoNing, Anshan, China |

Department of Chemistry, University of Southern California, Los Angeles, USA |

Publication type: Journal Article

Publication date: 2018-03-28

Springer Nature

Journal: Nature Communications

Quartile SCImago

Quartile WOS

Impact factor: 16.6

ISSN: 20411723, 20411723

DOI: 10.1038/s41467-018-03678-y

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PubMed ID: 29593262

General Chemistry

General Biochemistry, Genetics and Molecular Biology

General Physics and Astronomy

Abstract

The pentazolate anion, as a polynitrogen species, holds great promise as a high-energy density material for explosive or propulsion applications. Designing pentazole complexes that contain minimal non-energetic components is desirable in order to increase the material’s energy density. Here, we report a solvent-free pentazolate complex, AgN5, and a 3D energetic-framework, [Ag(NH3)2]+[Ag3(N5)4]ˉ, constructed from silver and cyclo-N5ˉ. The complexes are stable up to 90 °C and only Ag and N2 are observed as the final decomposition products. Efforts to isolate pure AgN5 were unsuccessful due to partial photolytical and/or thermal-decomposition to AgN3. Convincing evidence for the formation of AgN5 as the original reaction product is presented. The isolation of a cyclo-N5ˉ complex, devoid of stabilizing molecules and ions, such as H2O, H3O+, and NH4+, constitutes a major advance in pentazole chemistry. The pentazolate anion shows great promise for high energy density materials, but has only been isolated alongside non-energetic counter ions that impede its energetic properties. Here, the authors synthesize a silver cyclo-N5-complex devoid of stabilizing ions, as well as a complementary [Ag(NH3)2]+[Ag3(N5)4]− 3D framework.

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Citations by journals

	2 4 6 8 10
Crystal Growth and Design	Crystal Growth and Design, 10, 8% Crystal Growth and Design 10 publications, 8%
Inorganic Chemistry	Inorganic Chemistry, 7, 5.6% Inorganic Chemistry 7 publications, 5.6%
CrystEngComm	CrystEngComm, 7, 5.6% CrystEngComm 7 publications, 5.6%
Journal of Physical Chemistry C	Journal of Physical Chemistry C, 6, 4.8% Journal of Physical Chemistry C 6 publications, 4.8%
Journal of Physical Chemistry Letters	Journal of Physical Chemistry Letters, 5, 4% Journal of Physical Chemistry Letters 5 publications, 4%
Dalton Transactions	Dalton Transactions, 5, 4% Dalton Transactions 5 publications, 4%
Journal of Physical Chemistry A	Journal of Physical Chemistry A, 4, 3.2% Journal of Physical Chemistry A 4 publications, 3.2%
Physical Chemistry Chemical Physics	Physical Chemistry Chemical Physics, 4, 3.2% Physical Chemistry Chemical Physics 4 publications, 3.2%
Science China Materials	Science China Materials, 3, 2.4% Science China Materials 3 publications, 2.4%
Chemical Engineering Journal	Chemical Engineering Journal, 3, 2.4% Chemical Engineering Journal 3 publications, 2.4%
Angewandte Chemie - International Edition	Angewandte Chemie - International Edition, 3, 2.4% Angewandte Chemie - International Edition 3 publications, 2.4%
Angewandte Chemie	Angewandte Chemie, 3, 2.4% Angewandte Chemie 3 publications, 2.4%
Journal of the American Chemical Society	Journal of the American Chemical Society, 3, 2.4% Journal of the American Chemical Society 3 publications, 2.4%
New Journal of Chemistry	New Journal of Chemistry, 3, 2.4% New Journal of Chemistry 3 publications, 2.4%
Molecules	Molecules, 2, 1.6% Molecules 2 publications, 1.6%
Nature Chemistry	Nature Chemistry, 2, 1.6% Nature Chemistry 2 publications, 1.6%
FirePhysChem	FirePhysChem, 2, 1.6% FirePhysChem 2 publications, 1.6%
Energetic Materials Frontiers	Energetic Materials Frontiers, 2, 1.6% Energetic Materials Frontiers 2 publications, 1.6%
Engineering	Engineering, 2, 1.6% Engineering 2 publications, 1.6%
Chemistry - An Asian Journal	Chemistry - An Asian Journal, 2, 1.6% Chemistry - An Asian Journal 2 publications, 1.6%
International Journal of Quantum Chemistry	International Journal of Quantum Chemistry, 2, 1.6% International Journal of Quantum Chemistry 2 publications, 1.6%
Zeitschrift fur Anorganische und Allgemeine Chemie	Zeitschrift fur Anorganische und Allgemeine Chemie, 2, 1.6% Zeitschrift fur Anorganische und Allgemeine Chemie 2 publications, 1.6%
Chemistry of Materials	Chemistry of Materials, 2, 1.6% Chemistry of Materials 2 publications, 1.6%
Journal of Materials Chemistry A	Journal of Materials Chemistry A, 2, 1.6% Journal of Materials Chemistry A 2 publications, 1.6%
Chemistry - A European Journal	Chemistry - A European Journal, 1, 0.8% Chemistry - A European Journal 1 publication, 0.8%
ChemPlusChem	ChemPlusChem, 1, 0.8% ChemPlusChem 1 publication, 0.8%
Chemical Reviews	Chemical Reviews, 1, 0.8% Chemical Reviews 1 publication, 0.8%
AIP Advances	AIP Advances, 1, 0.8% AIP Advances 1 publication, 0.8%
Royal Society Open Science	Royal Society Open Science, 1, 0.8% Royal Society Open Science 1 publication, 0.8%
	2 4 6 8 10

Citations by publishers

	5 10 15 20 25 30 35 40 45
American Chemical Society (ACS)	American Chemical Society (ACS), 41, 32.8% American Chemical Society (ACS) 41 publications, 32.8%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 22, 17.6% Royal Society of Chemistry (RSC) 22 publications, 17.6%
Wiley	Wiley, 21, 16.8% Wiley 21 publications, 16.8%
Elsevier	Elsevier, 18, 14.4% Elsevier 18 publications, 14.4%
Springer Nature	Springer Nature, 11, 8.8% Springer Nature 11 publications, 8.8%
IOP Publishing	IOP Publishing, 3, 2.4% IOP Publishing 3 publications, 2.4%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 2, 1.6% Multidisciplinary Digital Publishing Institute (MDPI) 2 publications, 1.6%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 2, 1.6% American Institute of Physics (AIP) 2 publications, 1.6%
The Royal Society	The Royal Society, 1, 0.8% The Royal Society 1 publication, 0.8%
Taylor & Francis	Taylor & Francis, 1, 0.8% Taylor & Francis 1 publication, 0.8%
American Association for the Advancement of Science (AAAS)	American Association for the Advancement of Science (AAAS), 1, 0.8% American Association for the Advancement of Science (AAAS) 1 publication, 0.8%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 0.8% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 0.8%
	5 10 15 20 25 30 35 40 45

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GOST Copy

Sun C. et al. Synthesis of AgN5 and its extended 3D energetic framework // Nature Communications. 2018. Vol. 9. No. 1. 1269

GOST all authors (up to 50) Copy

Sun C., Zhang C., Jiang C., Yang C., Du Y., Zhao Y., Hu B., Zheng Z., Christe K. O. Synthesis of AgN5 and its extended 3D energetic framework // Nature Communications. 2018. Vol. 9. No. 1. 1269

RIS |

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RIS Copy

TY - JOUR

DO - 10.1038/s41467-018-03678-y

UR - https://doi.org/10.1038/s41467-018-03678-y

TI - Synthesis of AgN5 and its extended 3D energetic framework

T2 - Nature Communications

AU - Sun, Chengguo

AU - Zhang, Chong

AU - Jiang, Chao

AU - Yang, Chen

AU - Du, Yang

AU - Zhao, Yue

AU - Hu, Bingcheng

AU - Zheng, Zhansheng

AU - Christe, Karl O.

PY - 2018

DA - 2018/03/28 00:00:00

PB - Springer Nature

IS - 1

VL - 9

PMID - 29593262

SN - 2041-1723

ER -

BibTex

Cite this

BibTex Copy

@article{2018_Sun,

author = {Chengguo Sun and Chong Zhang and Chao Jiang and Chen Yang and Yang Du and Yue Zhao and Bingcheng Hu and Zhansheng Zheng and Karl O. Christe},

title = {Synthesis of AgN5 and its extended 3D energetic framework},

journal = {Nature Communications},

year = {2018},

volume = {9},

publisher = {Springer Nature},

month = {mar},

url = {https://doi.org/10.1038/s41467-018-03678-y},

number = {1},

doi = {10.1038/s41467-018-03678-y}

}

Found error?

Publisher

Springer Nature

Journal

Nature Communications

Quartile SCImago

Quartile WOS

Impact factor

16.6

ISSN

20411723 (Print)
20411723 (Electronic)