Open Access

Nature Communications, volume 9, issue 1, publication number 2756

Fe-N system at high pressure reveals a compound featuring polymeric nitrogen chains

Maxim Bykov ¹

E. Bykova ^{1, 2}

Georgios Aprilis ³

K. Glazyrin ²

E Koemets ¹

Irina Chuvashova ^{1, 3}

I Kupenko ⁴

C. McCammon ¹

M. Mezouar ⁵

V. Prakapenka ⁶

H.-P. Liermann ²

F. Tasnádi ^{7, 8}

A V Ponomareva ⁸

I A Abrikosov ⁷

N.A. Dubrovinskaia ³

L. Dubrovinsky ¹

Hide authors affiliations Show authors affiliations: 8 affiliations

Bayerisches GeoInstitut, University of Bayreuth, Bayreuth, Germany |

Photon Science, Deutsches Elektronen-Synchrotron, Hamburg, Germany |

Material Physics and Technology at Extreme Conditions, Laboratory of Crystallography, University of Bayreuth, Bayreuth, Germany |

⁴

Institut für Mineralogie, University of Münster, Münster, Germany |

⁵

European Synchrotron Radiation Facility, Grenoble cedex, France |

⁶

Center for Advanced Radiation Sources, University of Chicago, Argonne, USA |

⁷

Department of Physics, Chemistry and Biology (IFM), Linköping University, Linköping, Sweden |

⁸

Materials Modeling and Development Laboratory, National University of Science and Technology ‘MISIS’, Moscow, Russia |

Publication type: Journal Article

Publication date: 2018-07-16

Springer Nature

Journal: Nature Communications

Quartile SCImago

Quartile WOS

Impact factor: 16.6

ISSN: 20411723, 20411723

DOI: 10.1038/s41467-018-05143-2

Copy DOI

PubMed ID: 30013071

General Chemistry

General Biochemistry, Genetics and Molecular Biology

General Physics and Astronomy

Abstract

Poly-nitrogen compounds have been considered as potential high energy density materials for a long time due to the large number of energetic N–N or N=N bonds. In most cases high nitrogen content and stability at ambient conditions are mutually exclusive, thereby making the synthesis of such materials challenging. One way to stabilize such compounds is the application of high pressure. Here, through a direct reaction between Fe and N2 in a laser-heated diamond anvil cell, we synthesize three ironnitrogen compounds Fe3N2, FeN2 and FeN4. Their crystal structures are revealed by single-crystal synchrotron X-ray diffraction. Fe3N2, synthesized at 50 GPa, is isostructural to chromium carbide Cr3C2. FeN2 has a marcasite structure type and features covalently bonded dinitrogen units in its crystal structure. FeN4, synthesized at 106 GPa, features polymeric nitrogen chains of [N42−]n units. Based on results of structural studies and theoretical analysis, [N42−]n units in this compound reveal catena-poly[tetraz-1-ene-1,4-diyl] anions.Owing to the energetic nature of N–N bonds, poly-nitrogen compounds are considered promising high energy density materials. Here, the authors synthesize three iron–nitrogen compounds at high pressure, including FeN4, which features polymeric nitrogen chains of [N42−]n units.

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Inorganic Chemistry	Inorganic Chemistry, 10, 6.06% Inorganic Chemistry 10 publications, 6.06%
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Journal of Physics Condensed Matter	Journal of Physics Condensed Matter, 5, 3.03% Journal of Physics Condensed Matter 5 publications, 3.03%
Angewandte Chemie - International Edition	Angewandte Chemie - International Edition, 5, 3.03% Angewandte Chemie - International Edition 5 publications, 3.03%
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Chemical Communications	Chemical Communications, 4, 2.42% Chemical Communications 4 publications, 2.42%
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Crystal Growth and Design	Crystal Growth and Design, 3, 1.82% Crystal Growth and Design 3 publications, 1.82%
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Physical Review Materials	Physical Review Materials, 2, 1.21% Physical Review Materials 2 publications, 1.21%
Ceramics International	Ceramics International, 2, 1.21% Ceramics International 2 publications, 1.21%
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Physics Letters, Section A: General, Atomic and Solid State Physics	Physics Letters, Section A: General, Atomic and Solid State Physics, 2, 1.21% Physics Letters, Section A: General, Atomic and Solid State Physics 2 publications, 1.21%
ACS Nano	ACS Nano, 2, 1.21% ACS Nano 2 publications, 1.21%
Journal of the American Chemical Society	Journal of the American Chemical Society, 2, 1.21% Journal of the American Chemical Society 2 publications, 1.21%
Chemical Reviews	Chemical Reviews, 1, 0.61% Chemical Reviews 1 publication, 0.61%
Physical Review Letters	Physical Review Letters, 1, 0.61% Physical Review Letters 1 publication, 0.61%
Journal of Geophysical Research: Solid Earth	Journal of Geophysical Research: Solid Earth, 1, 0.61% Journal of Geophysical Research: Solid Earth 1 publication, 0.61%
	2 4 6 8 10

Citations by publishers

	5 10 15 20 25 30 35 40 45
American Chemical Society (ACS)	American Chemical Society (ACS), 42, 25.45% American Chemical Society (ACS) 42 publications, 25.45%
Wiley	Wiley, 26, 15.76% Wiley 26 publications, 15.76%
Elsevier	Elsevier, 24, 14.55% Elsevier 24 publications, 14.55%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 17, 10.3% Royal Society of Chemistry (RSC) 17 publications, 10.3%
Springer Nature	Springer Nature, 11, 6.67% Springer Nature 11 publications, 6.67%
American Physical Society (APS)	American Physical Society (APS), 10, 6.06% American Physical Society (APS) 10 publications, 6.06%
IOP Publishing	IOP Publishing, 10, 6.06% IOP Publishing 10 publications, 6.06%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 8, 4.85% American Institute of Physics (AIP) 8 publications, 4.85%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 5, 3.03% Multidisciplinary Digital Publishing Institute (MDPI) 5 publications, 3.03%
Taylor & Francis	Taylor & Francis, 2, 1.21% Taylor & Francis 2 publications, 1.21%
International Union of Crystallography (IUCr)	International Union of Crystallography (IUCr), 1, 0.61% International Union of Crystallography (IUCr) 1 publication, 0.61%
World Scientific	World Scientific, 1, 0.61% World Scientific 1 publication, 0.61%
Frontiers Media S.A.	Frontiers Media S.A., 1, 0.61% Frontiers Media S.A. 1 publication, 0.61%
Japan Society of Applied Physics	Japan Society of Applied Physics, 1, 0.61% Japan Society of Applied Physics 1 publication, 0.61%
Materials Research Society	Materials Research Society, 1, 0.61% Materials Research Society 1 publication, 0.61%
OAE Publishing Inc.	OAE Publishing Inc., 1, 0.61% OAE Publishing Inc. 1 publication, 0.61%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 0.61% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 0.61%
	5 10 15 20 25 30 35 40 45

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Bykov M. et al. Fe-N system at high pressure reveals a compound featuring polymeric nitrogen chains // Nature Communications. 2018. Vol. 9. No. 1. 2756

GOST all authors (up to 50) Copy

Bykov M., Bykova E., Aprilis G., Glazyrin K., Koemets E., Chuvashova I., Kupenko I., McCammon C., Mezouar M., Prakapenka V., Liermann H., Tasnádi F., Ponomareva A. V., Abrikosov I. A., Dubrovinskaia N., Dubrovinsky L. Fe-N system at high pressure reveals a compound featuring polymeric nitrogen chains // Nature Communications. 2018. Vol. 9. No. 1. 2756

RIS |

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RIS Copy

TY - JOUR

DO - 10.1038/s41467-018-05143-2

UR - https://doi.org/10.1038/s41467-018-05143-2

TI - Fe-N system at high pressure reveals a compound featuring polymeric nitrogen chains

T2 - Nature Communications

AU - Bykov, Maxim

AU - Bykova, E.

AU - Aprilis, Georgios

AU - Glazyrin, K.

AU - Koemets, E

AU - Chuvashova, Irina

AU - Kupenko, I

AU - McCammon, C.

AU - Mezouar, M.

AU - Prakapenka, V.

AU - Liermann, H.-P.

AU - Tasnádi, F.

AU - Ponomareva, A V

AU - Abrikosov, I A

AU - Dubrovinskaia, N.A.

AU - Dubrovinsky, L.

PY - 2018

DA - 2018/07/16 00:00:00

PB - Springer Nature

IS - 1

VL - 9

PMID - 30013071

SN - 2041-1723

ER -

BibTex

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@article{2018_Bykov,

author = {Maxim Bykov and E. Bykova and Georgios Aprilis and K. Glazyrin and E Koemets and Irina Chuvashova and I Kupenko and C. McCammon and M. Mezouar and V. Prakapenka and H.-P. Liermann and F. Tasnádi and A V Ponomareva and I A Abrikosov and N.A. Dubrovinskaia and L. Dubrovinsky},

title = {Fe-N system at high pressure reveals a compound featuring polymeric nitrogen chains},

journal = {Nature Communications},

year = {2018},

volume = {9},

publisher = {Springer Nature},

month = {jul},

url = {https://doi.org/10.1038/s41467-018-05143-2},

number = {1},

doi = {10.1038/s41467-018-05143-2}

}

Found error?

Publisher

Springer Nature

Journal

Nature Communications

Quartile SCImago

Quartile WOS

Impact factor

16.6

ISSN

20411723 (Print)
20411723 (Electronic)