Open Access

Nature Communications, volume 10, issue 1, publication number 4515

Synthesis of magnesium-nitrogen salts of polynitrogen anions

Dominique Laniel ¹

Bjoern Winkler ²

Egor Koemets ³

Timofey Fedotenko ¹

Maxim Bykov ³

E. Bykova ⁴

L. Dubrovinsky ³

N.A. Dubrovinskaia ¹

Hide authors affiliations Show authors affiliations: 4 affiliations

Material Physics and Technology at Extreme Conditions, Laboratory of Crystallography, University of Bayreuth, Bayreuth, Germany |

Institut für Geowissenschaften, Abteilung Kristallographie, Johann Wolfgang Goethe-Universität Frankfurt, Frankfurt am Main, Germany |

Bayerisches GeoInstitut, University of Bayreuth, Bayreuth, Germany |

⁴

Photon Science, Deutsches Elektronen-Synchrotron, Hamburg, Germany |

Publication type: Journal Article

Publication date: 2019-10-04

Springer Nature

Journal: Nature Communications

Quartile SCImago

Quartile WOS

Impact factor: 16.6

ISSN: 20411723, 20411723

DOI: 10.1038/s41467-019-12530-w

Copy DOI

PubMed ID: 31586062

General Chemistry

General Biochemistry, Genetics and Molecular Biology

General Physics and Astronomy

Abstract

The synthesis of polynitrogen compounds is of fundamental importance due to their potential as environmentally-friendly high energy density materials. Attesting to the intrinsic difficulties related to their formation, only three polynitrogen ions, bulk stabilized as salts, are known. Here, magnesium and molecular nitrogen are compressed to about 50 GPa and laser-heated, producing two chemically simple salts of polynitrogen anions, MgN4 and Mg2N4. Single-crystal X-ray diffraction reveals infinite anionic polythiazyl-like 1D N-N chains in the crystal structure of MgN4 and cis-tetranitrogen N44− units in the two isosymmetric polymorphs of Mg2N4. The cis-tetranitrogen units are found to be recoverable at atmospheric pressure. Our results respond to the quest for polynitrogen entities stable at ambient conditions, reveal the potential of employing high pressures in their synthesis and enrich the nitrogen chemistry through the discovery of other nitrogen species, which provides further possibilities to design improved polynitrogen arrangements. Polynitrogen compounds are potentially promising high energy density materials, but are difficult to synthesize due to their instability. Here, the authors observe the formation, under high pressure, of a Mg2N4 magnesium–tetranitrogen salt which remains stable at ambient conditions.

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Inorganic Chemistry	Inorganic Chemistry, 6, 6.67% Inorganic Chemistry 6 publications, 6.67%
Physical Chemistry Chemical Physics	Physical Chemistry Chemical Physics, 6, 6.67% Physical Chemistry Chemical Physics 6 publications, 6.67%
Physical Review B	Physical Review B, 4, 4.44% Physical Review B 4 publications, 4.44%
Angewandte Chemie - International Edition	Angewandte Chemie - International Edition, 4, 4.44% Angewandte Chemie - International Edition 4 publications, 4.44%
Angewandte Chemie	Angewandte Chemie, 4, 4.44% Angewandte Chemie 4 publications, 4.44%
Journal of Physical Chemistry C	Journal of Physical Chemistry C, 4, 4.44% Journal of Physical Chemistry C 4 publications, 4.44%
Journal of the American Chemical Society	Journal of the American Chemical Society, 3, 3.33% Journal of the American Chemical Society 3 publications, 3.33%
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Journal of Physics Condensed Matter	Journal of Physics Condensed Matter, 3, 3.33% Journal of Physics Condensed Matter 3 publications, 3.33%
Physica Status Solidi (B): Basic Research	Physica Status Solidi (B): Basic Research, 3, 3.33% Physica Status Solidi (B): Basic Research 3 publications, 3.33%
Journal of Physical Chemistry Letters	Journal of Physical Chemistry Letters, 3, 3.33% Journal of Physical Chemistry Letters 3 publications, 3.33%
Nature Chemistry	Nature Chemistry, 2, 2.22% Nature Chemistry 2 publications, 2.22%
Physical Review Letters	Physical Review Letters, 2, 2.22% Physical Review Letters 2 publications, 2.22%
Communications Chemistry	Communications Chemistry, 2, 2.22% Communications Chemistry 2 publications, 2.22%
Chinese Physics B	Chinese Physics B, 2, 2.22% Chinese Physics B 2 publications, 2.22%
Chemistry - A European Journal	Chemistry - A European Journal, 2, 2.22% Chemistry - A European Journal 2 publications, 2.22%
Review of Scientific Instruments	Review of Scientific Instruments, 1, 1.11% Review of Scientific Instruments 1 publication, 1.11%
IUCrJ	IUCrJ, 1, 1.11% IUCrJ 1 publication, 1.11%
Materials	Materials, 1, 1.11% Materials 1 publication, 1.11%
Nature Reviews Chemistry	Nature Reviews Chemistry, 1, 1.11% Nature Reviews Chemistry 1 publication, 1.11%
Science China: Physics, Mechanics and Astronomy	Science China: Physics, Mechanics and Astronomy, 1, 1.11% Science China: Physics, Mechanics and Astronomy 1 publication, 1.11%
Chemical Engineering Journal	Chemical Engineering Journal, 1, 1.11% Chemical Engineering Journal 1 publication, 1.11%
Materials Science and Engineering B: Solid-State Materials for Advanced Technology	Materials Science and Engineering B: Solid-State Materials for Advanced Technology, 1, 1.11% Materials Science and Engineering B: Solid-State Materials for Advanced Technology 1 publication, 1.11%
Materials Science in Semiconductor Processing	Materials Science in Semiconductor Processing, 1, 1.11% Materials Science in Semiconductor Processing 1 publication, 1.11%
Physica Scripta	Physica Scripta, 1, 1.11% Physica Scripta 1 publication, 1.11%
Chinese Physics Letters	Chinese Physics Letters, 1, 1.11% Chinese Physics Letters 1 publication, 1.11%
Chemical Physics Letters	Chemical Physics Letters, 1, 1.11% Chemical Physics Letters 1 publication, 1.11%
European Journal of Inorganic Chemistry	European Journal of Inorganic Chemistry, 1, 1.11% European Journal of Inorganic Chemistry 1 publication, 1.11%
Journal of Physical Organic Chemistry	Journal of Physical Organic Chemistry, 1, 1.11% Journal of Physical Organic Chemistry 1 publication, 1.11%
Materials Advances	Materials Advances, 1, 1.11% Materials Advances 1 publication, 1.11%
	1 2 3 4 5 6

Citations by publishers

	2 4 6 8 10 12 14 16 18 20
Wiley	Wiley, 19, 21.11% Wiley 19 publications, 21.11%
American Chemical Society (ACS)	American Chemical Society (ACS), 17, 18.89% American Chemical Society (ACS) 17 publications, 18.89%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 11, 12.22% Royal Society of Chemistry (RSC) 11 publications, 12.22%
Elsevier	Elsevier, 9, 10% Elsevier 9 publications, 10%
American Physical Society (APS)	American Physical Society (APS), 8, 8.89% American Physical Society (APS) 8 publications, 8.89%
American Institute of Physics (AIP)	American Institute of Physics (AIP), 7, 7.78% American Institute of Physics (AIP) 7 publications, 7.78%
IOP Publishing	IOP Publishing, 7, 7.78% IOP Publishing 7 publications, 7.78%
Springer Nature	Springer Nature, 6, 6.67% Springer Nature 6 publications, 6.67%
International Union of Crystallography (IUCr)	International Union of Crystallography (IUCr), 1, 1.11% International Union of Crystallography (IUCr) 1 publication, 1.11%
Multidisciplinary Digital Publishing Institute (MDPI)	Multidisciplinary Digital Publishing Institute (MDPI), 1, 1.11% Multidisciplinary Digital Publishing Institute (MDPI) 1 publication, 1.11%
Science in China Press	Science in China Press, 1, 1.11% Science in China Press 1 publication, 1.11%
OAE Publishing Inc.	OAE Publishing Inc., 1, 1.11% OAE Publishing Inc. 1 publication, 1.11%
Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii	Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii, 1, 1.11% Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii 1 publication, 1.11%
	2 4 6 8 10 12 14 16 18 20

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Laniel D. et al. Synthesis of magnesium-nitrogen salts of polynitrogen anions // Nature Communications. 2019. Vol. 10. No. 1. 4515

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Laniel D., Winkler B., Koemets E., Fedotenko T., Bykov M., Bykova E., Dubrovinsky L., Dubrovinskaia N. Synthesis of magnesium-nitrogen salts of polynitrogen anions // Nature Communications. 2019. Vol. 10. No. 1. 4515

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RIS Copy

TY - JOUR

DO - 10.1038/s41467-019-12530-w

UR - https://doi.org/10.1038/s41467-019-12530-w

TI - Synthesis of magnesium-nitrogen salts of polynitrogen anions

T2 - Nature Communications

AU - Laniel, Dominique

AU - Winkler, Bjoern

AU - Koemets, Egor

AU - Fedotenko, Timofey

AU - Bykov, Maxim

AU - Bykova, E.

AU - Dubrovinsky, L.

AU - Dubrovinskaia, N.A.

PY - 2019

DA - 2019/10/04 00:00:00

PB - Springer Nature

IS - 1

VL - 10

PMID - 31586062

SN - 2041-1723

ER -

BibTex

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BibTex Copy

@article{2019_Laniel,

author = {Dominique Laniel and Bjoern Winkler and Egor Koemets and Timofey Fedotenko and Maxim Bykov and E. Bykova and L. Dubrovinsky and N.A. Dubrovinskaia},

title = {Synthesis of magnesium-nitrogen salts of polynitrogen anions},

journal = {Nature Communications},

year = {2019},

volume = {10},

publisher = {Springer Nature},

month = {oct},

url = {https://doi.org/10.1038/s41467-019-12530-w},

number = {1},

doi = {10.1038/s41467-019-12530-w}

}

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Springer Nature

Journal

Nature Communications

Quartile SCImago

Quartile WOS

Impact factor

16.6

ISSN

20411723 (Print)
20411723 (Electronic)