One-pot synthesis of pillar[n]arenes catalyzed by a minimum amount of TfOH and a solution-phase mechanistic study.
Publication type: Journal Article
Publication date: 2012-10-16
scimago Q2
wos Q2
SJR: 0.600
CiteScore: 5.2
Impact factor: 2.7
ISSN: 14770520, 14770539
PubMed ID:
23108705
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
A practical and effective trifluoromethanesulfonic acid (TfOH)-catalyzed cyclooligomerization strategy was developed for the synthesis of functionalized pillar[n]arenes and copillar[5]arenes from 1,4-dialkoxybenzenes with paraformaldehyde under mild reaction conditions, and the reaction mechanism of solution-phase catalytic synthesis of pillararenes was investigated by room-temperature X-band ESR spectroscopy, mass spectroscopy, NMR and control experiments, suggesting a free radical process initially and a Friedel-Crafts alkylation process during the consequent coupling and ring-closure stage.
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Metrics
94
Total citations:
94
Citations from 2024:
6
(6%)
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MLA
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GOST
Copy
Wang K. et al. One-pot synthesis of pillar[n]arenes catalyzed by a minimum amount of TfOH and a solution-phase mechanistic study. // Organic and Biomolecular Chemistry. 2012. Vol. 10. No. 47. p. 9405.
GOST all authors (up to 50)
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Wang K., TAN L. L., Tan L., Chen D., Song N., Guan X., Zhang S. X., Li C., Yang Y. One-pot synthesis of pillar[n]arenes catalyzed by a minimum amount of TfOH and a solution-phase mechanistic study. // Organic and Biomolecular Chemistry. 2012. Vol. 10. No. 47. p. 9405.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1039/c2ob26635k
UR - https://doi.org/10.1039/c2ob26635k
TI - One-pot synthesis of pillar[n]arenes catalyzed by a minimum amount of TfOH and a solution-phase mechanistic study.
T2 - Organic and Biomolecular Chemistry
AU - Wang, Kai
AU - TAN, LI LI
AU - Tan, Li-Li
AU - Chen, Dai-Xiong
AU - Song, Nan
AU - Guan, Xi
AU - Zhang, Sean Xiao-An
AU - Li, Chunju
AU - Yang, Ying-Wei
PY - 2012
DA - 2012/10/16
PB - Royal Society of Chemistry (RSC)
SP - 9405
IS - 47
VL - 10
PMID - 23108705
SN - 1477-0520
SN - 1477-0539
ER -
Cite this
BibTex (up to 50 authors)
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@article{2012_Wang,
author = {Kai Wang and LI LI TAN and Li-Li Tan and Dai-Xiong Chen and Nan Song and Xi Guan and Sean Xiao-An Zhang and Chunju Li and Ying-Wei Yang},
title = {One-pot synthesis of pillar[n]arenes catalyzed by a minimum amount of TfOH and a solution-phase mechanistic study.},
journal = {Organic and Biomolecular Chemistry},
year = {2012},
volume = {10},
publisher = {Royal Society of Chemistry (RSC)},
month = {oct},
url = {https://doi.org/10.1039/c2ob26635k},
number = {47},
pages = {9405},
doi = {10.1039/c2ob26635k}
}
Cite this
MLA
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Wang, Kai, et al. “One-pot synthesis of pillar[n]arenes catalyzed by a minimum amount of TfOH and a solution-phase mechanistic study..” Organic and Biomolecular Chemistry, vol. 10, no. 47, Oct. 2012, p. 9405. https://doi.org/10.1039/c2ob26635k.