Open Access
15N labeling and analysis of 13C–15N and 1H–15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles
Sergey Deev
1, 2, 3, 4, 5, 6, 7
,
Tatyana S Shestakova
1, 3, 4, 5
,
Valery Charushin
1, 2
,
Valery N. Charushin
3, 4, 5, 6, 7
,
O. N. Chupakhin
1, 2, 3, 4, 5, 6, 7
4
620002 Yekaterinburg
|
5
RUSSIAN FEDERATION
|
7
620219 Yekaterinburg
|
Publication type: Journal Article
Publication date: 2019-08-28
scimago Q1
wos Q2
SJR: 0.777
CiteScore: 7.6
Impact factor: 4.6
ISSN: 20462069
PubMed ID:
35528595
General Chemistry
General Chemical Engineering
Abstract
This review provides a generalization of effective examples of 15N labeling followed by an analysis of 13C-15N (JCN) and 1H-15N (JHN) coupling constants in solution as a tool to study the structural aspects and pathways of chemical transformations (e.g., rearrangements and ring-chain tautomerisms) in monocyclic and fused nitrogen heterocycles. This approach allows us to significantly expand and supplement the scope of NMR techniques for heterocyclic compounds. Moreover, methods for the incorporation of 15N atoms into the cores of various N-heterocycles have been collected in this work.
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35
Total citations:
35
Citations from 2025:
6
(17.14%)
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GOST
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Deev S. et al. 15N labeling and analysis of 13C–15N and 1H–15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles // RSC Advances. 2019. Vol. 9. No. 46. pp. 26856-26879.
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Deev S., Khalymbadzha I. A., Shestakova T. S., Charushin V., Charushin V. N., Chupakhin O. N. 15N labeling and analysis of 13C–15N and 1H–15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles // RSC Advances. 2019. Vol. 9. No. 46. pp. 26856-26879.
Cite this
RIS
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TY - JOUR
DO - 10.1039/C9RA04825A
UR - https://xlink.rsc.org/?DOI=C9RA04825A
TI - 15N labeling and analysis of 13C–15N and 1H–15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles
T2 - RSC Advances
AU - Deev, Sergey
AU - Khalymbadzha, Igor A
AU - Shestakova, Tatyana S
AU - Charushin, Valery
AU - Charushin, Valery N.
AU - Chupakhin, O. N.
PY - 2019
DA - 2019/08/28
PB - Royal Society of Chemistry (RSC)
SP - 26856-26879
IS - 46
VL - 9
PMID - 35528595
SN - 2046-2069
ER -
Cite this
BibTex (up to 50 authors)
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@article{2019_Deev,
author = {Sergey Deev and Igor A Khalymbadzha and Tatyana S Shestakova and Valery Charushin and Valery N. Charushin and O. N. Chupakhin},
title = {15N labeling and analysis of 13C–15N and 1H–15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles},
journal = {RSC Advances},
year = {2019},
volume = {9},
publisher = {Royal Society of Chemistry (RSC)},
month = {aug},
url = {https://xlink.rsc.org/?DOI=C9RA04825A},
number = {46},
pages = {26856--26879},
doi = {10.1039/C9RA04825A}
}
Cite this
MLA
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Deev, Sergey, et al. “15N labeling and analysis of 13C–15N and 1H–15N couplings in studies of the structures and chemical transformations of nitrogen heterocycles.” RSC Advances, vol. 9, no. 46, Aug. 2019, pp. 26856-26879. https://xlink.rsc.org/?DOI=C9RA04825A.