Different fluoride anion sources and (trifluoromethyl)trimethylsilane: molecular structure of tris(dimethylamino)sulfonium bis(trifluoromethyl)trimethylsiliconate, the first isolated pentacoordinate silicon species with five Si–C bonds
Тип публикации: Journal Article
Дата публикации: 1999-01-01
scimago Q1
wos Q2
БС1
SJR: 1.037
CiteScore: 7.4
Impact factor: 4.2
ISSN: 13597345, 1364548X
Materials Chemistry
Metals and Alloys
Surfaces, Coatings and Films
General Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Catalysis
Краткое описание
(Trifluoromethyl)trimethylsilane, CF3SiMe3 reacts with [(Me2N)3S]+[Me3SiF2]–, Q+F– and Q+[HF2]– (Q+ = Me4N+, [(Me2N)3C]+, [(Me2N)4P]+) at –70 to 50 °C to afford the first hypervalent silicon species, [(CF3)2SiMe3]– with five Si–C bonds (stable in monoglyme up to –10 °C) as the main reactive species whose molecular structure was determined by X-ray crystallography.
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Kolomeitsev A. et al. Different fluoride anion sources and (trifluoromethyl)trimethylsilane: molecular structure of tris(dimethylamino)sulfonium bis(trifluoromethyl)trimethylsiliconate, the first isolated pentacoordinate silicon species with five Si–C bonds // Chemical Communications. 1999. Vol. 11. pp. 1017-1018.
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Kolomeitsev A., Movchun V., Rusanov E. B., Bissky G., Lork E., Röschenthaler G., Kirsch P. Different fluoride anion sources and (trifluoromethyl)trimethylsilane: molecular structure of tris(dimethylamino)sulfonium bis(trifluoromethyl)trimethylsiliconate, the first isolated pentacoordinate silicon species with five Si–C bonds // Chemical Communications. 1999. Vol. 11. pp. 1017-1018.
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TY - JOUR
DO - 10.1039/a901953g
UR - https://doi.org/10.1039/a901953g
TI - Different fluoride anion sources and (trifluoromethyl)trimethylsilane: molecular structure of tris(dimethylamino)sulfonium bis(trifluoromethyl)trimethylsiliconate, the first isolated pentacoordinate silicon species with five Si–C bonds
T2 - Chemical Communications
AU - Kolomeitsev, Alexander
AU - Movchun, Valery
AU - Rusanov, Eduard B.
AU - Bissky, German
AU - Lork, Enno
AU - Röschenthaler, Gerd-Volker
AU - Kirsch, Peer
PY - 1999
DA - 1999/01/01
PB - Royal Society of Chemistry (RSC)
SP - 1017-1018
IS - 11
SN - 1359-7345
SN - 1364-548X
ER -
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@article{1999_Kolomeitsev,
author = {Alexander Kolomeitsev and Valery Movchun and Eduard B. Rusanov and German Bissky and Enno Lork and Gerd-Volker Röschenthaler and Peer Kirsch},
title = {Different fluoride anion sources and (trifluoromethyl)trimethylsilane: molecular structure of tris(dimethylamino)sulfonium bis(trifluoromethyl)trimethylsiliconate, the first isolated pentacoordinate silicon species with five Si–C bonds},
journal = {Chemical Communications},
year = {1999},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/a901953g},
number = {11},
pages = {1017--1018},
doi = {10.1039/a901953g}
}