Synthesis and reactions of Biginelli-compounds. Part 23. Chemoenzymatic syntheses of enanttiomerically pure 4-aryl-3,4-dihydropyrimidin-2(1H)-ones
Тип публикации: Journal Article
Дата публикации: 2000-01-01
SJR: —
CiteScore: —
Impact factor: —
ISSN: 0300922X, 13645463, 14727781
General Medicine
Краткое описание
Enantiomerically pure dihydropyrimidones (DHPMs) were prepared by lipase-catalyzed enzymatic resolution of two types of activated DHPM esters. In the first model series, pivaloyloxymethyl-activated DHPM C5-esters 10a–c were resolved on an analytical scale by various lipases in two different solvent systems with selectivities E 200) to furnish, after deprotection, DHPMs (R)- and (S)-13 on a semi-preparative scale. Treatment of (R)-13 with trichloroacetyl isocyanate produced the antihypertensive agent (R)-SQ 32926.
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Schnell B. et al. Synthesis and reactions of Biginelli-compounds. Part 23. Chemoenzymatic syntheses of enanttiomerically pure 4-aryl-3,4-dihydropyrimidin-2(1H)-ones // Journal of the Chemical Society Perkin Transactions 1. 2000. Vol. 24. pp. 4382-4389.
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Schnell B., Krenn W., Faber K., Kappe C. Synthesis and reactions of Biginelli-compounds. Part 23. Chemoenzymatic syntheses of enanttiomerically pure 4-aryl-3,4-dihydropyrimidin-2(1H)-ones // Journal of the Chemical Society Perkin Transactions 1. 2000. Vol. 24. pp. 4382-4389.
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TY - JOUR
DO - 10.1039/b006372j
UR - https://doi.org/10.1039/b006372j
TI - Synthesis and reactions of Biginelli-compounds. Part 23. Chemoenzymatic syntheses of enanttiomerically pure 4-aryl-3,4-dihydropyrimidin-2(1H)-ones
T2 - Journal of the Chemical Society Perkin Transactions 1
AU - Schnell, Barbara
AU - Krenn, Wolfram
AU - Faber, K.N
AU - Kappe, C.Oliver
PY - 2000
DA - 2000/01/01
PB - Royal Society of Chemistry (RSC)
SP - 4382-4389
IS - 24
SN - 0300-922X
SN - 1364-5463
SN - 1472-7781
ER -
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@article{2000_Schnell,
author = {Barbara Schnell and Wolfram Krenn and K.N Faber and C.Oliver Kappe},
title = {Synthesis and reactions of Biginelli-compounds. Part 23. Chemoenzymatic syntheses of enanttiomerically pure 4-aryl-3,4-dihydropyrimidin-2(1H)-ones},
journal = {Journal of the Chemical Society Perkin Transactions 1},
year = {2000},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/b006372j},
number = {24},
pages = {4382--4389},
doi = {10.1039/b006372j}
}