Crystalline binuclear cis- and trans-chlorotin(II ) amides [Sn(µ-Cl)(NR2)]2, the cis-1a ⇌trans-1b isomerisation for [NR2= NCMe2(CH2)3CMe2], and the X-ray structures of 1a and of trans-[Sn(µ-Cl){N(SiMe3)2}]2
Тип публикации: Journal Article
Дата публикации: 1991-01-01
SJR: —
CiteScore: —
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ISSN: 00224936
Molecular Medicine
Краткое описание
Crystalline binuclear chlorotin(II) amides [Sn(µ-Cl)(NR2)]2 have been X-ray characterised as cis-[NR2= [graphic omitted]Me2, 1a] and trans-(R = SiMe3, 2b) conformers [Cl–Sn–Cl′= 78.53(4)1a or 81.33(4)°2b, Sn–Cl–Sn′ 100.91(4)1a or 98.67(4)°2b, 2.74 1a or 2.67 A2b]; a solution of 1 in toluene undergoes rapid cis⇌trans exchange at ambient temperature, but distinct cis-1a and trans-1b forms coexist below 192 K (119Sn NMR spectroscopy and line-shape analysis) and evidence is presented for an intramolecular mechanism for this exchange.
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Chorley R. W. et al. Crystalline binuclear cis- and trans-chlorotin(II) amides [Sn(µ-Cl)(NR2)]2, the cis-1a ⇌trans-1b isomerisation for [NR2= NCMe2(CH2)3CMe2], and the X-ray structures of 1a and of trans-[Sn(µ-Cl){N(SiMe3)2}]2 // Journal of the Chemical Society Chemical Communications. 1991. Vol. 18. pp. 1302-1303.
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Chorley R. W., Hitchock P. B., Jolly B. S., Lappert M. F., Lawless G. A. Crystalline binuclear cis- and trans-chlorotin(II) amides [Sn(µ-Cl)(NR2)]2, the cis-1a ⇌trans-1b isomerisation for [NR2= NCMe2(CH2)3CMe2], and the X-ray structures of 1a and of trans-[Sn(µ-Cl){N(SiMe3)2}]2 // Journal of the Chemical Society Chemical Communications. 1991. Vol. 18. pp. 1302-1303.
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TY - JOUR
DO - 10.1039/c39910001302
UR - https://doi.org/10.1039/c39910001302
TI - Crystalline binuclear cis- and trans-chlorotin(II) amides [Sn(µ-Cl)(NR2)]2, the cis-1a ⇌trans-1b isomerisation for [NR2= NCMe2(CH2)3CMe2], and the X-ray structures of 1a and of trans-[Sn(µ-Cl){N(SiMe3)2}]2
T2 - Journal of the Chemical Society Chemical Communications
AU - Chorley, Richard W
AU - Hitchock, Peter B
AU - Jolly, Brian S
AU - Lappert, Michael F.
AU - Lawless, Gerard A
PY - 1991
DA - 1991/01/01
PB - Royal Society of Chemistry (RSC)
SP - 1302-1303
IS - 18
SN - 0022-4936
ER -
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@article{1991_Chorley,
author = {Richard W Chorley and Peter B Hitchock and Brian S Jolly and Michael F. Lappert and Gerard A Lawless},
title = {Crystalline binuclear cis- and trans-chlorotin(II) amides [Sn(µ-Cl)(NR2)]2, the cis-1a ⇌trans-1b isomerisation for [NR2= NCMe2(CH2)3CMe2], and the X-ray structures of 1a and of trans-[Sn(µ-Cl){N(SiMe3)2}]2},
journal = {Journal of the Chemical Society Chemical Communications},
year = {1991},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/c39910001302},
number = {18},
pages = {1302--1303},
doi = {10.1039/c39910001302}
}
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