Phosphomolybdic and phosphotungstic acids as efficient catalysts for the synthesis of bridged 1,2,4,5-tetraoxanes from β-diketones and hydrogen peroxide
Тип публикации: Journal Article
Дата публикации: 2013-02-14
scimago Q2
wos Q2
БС1
SJR: 0.600
CiteScore: 5.2
Impact factor: 2.7
ISSN: 14770520, 14770539
PubMed ID:
23446630
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Краткое описание
Phosphomolybdic acid (PMA) and phosphotungstic acid (PTA) efficiently catalyze the addition of H2O2 to β-diketones to form bridged 1,2,4,5-tetraoxanes. These reactions are not accompanied by the formation of monocyclic peroxides containing hydroxy and hydroperoxide groups or polymeric peroxides. The use of these catalysts made it possible to obtain bridged tetraoxanes from easily oxidizable benzoylacetone derivatives and α-unsubstituted β-diketones. The syntheses are scaled up to ten grams. The resulting peroxides can be easily isolated from the reaction mixture by column chromatography. The yield of tetraoxanes depends on the structure of β-diketone and varies from 12 to 83%. NMR monitoring of two bridged 1,2,4,5-tetraoxanes synthesis was carried out.
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Terent'ev A. O. et al. Phosphomolybdic and phosphotungstic acids as efficient catalysts for the synthesis of bridged 1,2,4,5-tetraoxanes from β-diketones and hydrogen peroxide // Organic and Biomolecular Chemistry. 2013. Vol. 11. No. 16. p. 2613.
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Terent'ev A. O., Yaremenko I. A., Vil’ V. A., Moiseev I. K., Konkov S. A., Dembitsky V. M., Levitsky D. O., Nikishin G. I. Phosphomolybdic and phosphotungstic acids as efficient catalysts for the synthesis of bridged 1,2,4,5-tetraoxanes from β-diketones and hydrogen peroxide // Organic and Biomolecular Chemistry. 2013. Vol. 11. No. 16. p. 2613.
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TY - JOUR
DO - 10.1039/c3ob27239g
UR - https://doi.org/10.1039/c3ob27239g
TI - Phosphomolybdic and phosphotungstic acids as efficient catalysts for the synthesis of bridged 1,2,4,5-tetraoxanes from β-diketones and hydrogen peroxide
T2 - Organic and Biomolecular Chemistry
AU - Terent'ev, Alexander O.
AU - Yaremenko, Ivan A
AU - Vil’, Vera A.
AU - Moiseev, Igor K
AU - Konkov, Sergey A
AU - Dembitsky, Valery M.
AU - Levitsky, Dmitri O.
AU - Nikishin, Gennady I.
PY - 2013
DA - 2013/02/14
PB - Royal Society of Chemistry (RSC)
SP - 2613
IS - 16
VL - 11
PMID - 23446630
SN - 1477-0520
SN - 1477-0539
ER -
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@article{2013_Terent'ev,
author = {Alexander O. Terent'ev and Ivan A Yaremenko and Vera A. Vil’ and Igor K Moiseev and Sergey A Konkov and Valery M. Dembitsky and Dmitri O. Levitsky and Gennady I. Nikishin},
title = {Phosphomolybdic and phosphotungstic acids as efficient catalysts for the synthesis of bridged 1,2,4,5-tetraoxanes from β-diketones and hydrogen peroxide},
journal = {Organic and Biomolecular Chemistry},
year = {2013},
volume = {11},
publisher = {Royal Society of Chemistry (RSC)},
month = {feb},
url = {https://doi.org/10.1039/c3ob27239g},
number = {16},
pages = {2613},
doi = {10.1039/c3ob27239g}
}
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Terent'ev, Alexander O., et al. “Phosphomolybdic and phosphotungstic acids as efficient catalysts for the synthesis of bridged 1,2,4,5-tetraoxanes from β-diketones and hydrogen peroxide.” Organic and Biomolecular Chemistry, vol. 11, no. 16, Feb. 2013, p. 2613. https://doi.org/10.1039/c3ob27239g.