Metal-free radical thiolations mediated by very weak bases
Publication type: Journal Article
Publication date: 2016-11-24
scimago Q2
wos Q2
SJR: 0.600
CiteScore: 5.2
Impact factor: 2.7
ISSN: 14770520, 14770539
PubMed ID:
27883150
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
Aromatic thioethers and analogous heavier chalcogenides were prepared by reaction of arene-diazonium salts with disulfides in the presence of the cheap and weak base NaOAc. The mild and practical reaction conditions (equimolar reagents, DMSO, r.t., 8 h) tolerate various functional groups (e.g. Br, Cl, NO2, CO2R, OH, SCF3, furans). Mechanistic studies indicate the operation of a radical aromatic substitution mechanism via aryl, acetyloxyl, thiyl, and dimsyl radicals.
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38
Total citations:
38
Citations from 2025:
3
(7.89%)
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GOST
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Koziakov D., Májek M., von Wangelin A. J. Metal-free radical thiolations mediated by very weak bases // Organic and Biomolecular Chemistry. 2016. Vol. 14. No. 48. pp. 11347-11352.
GOST all authors (up to 50)
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Koziakov D., Májek M., von Wangelin A. J. Metal-free radical thiolations mediated by very weak bases // Organic and Biomolecular Chemistry. 2016. Vol. 14. No. 48. pp. 11347-11352.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1039/c6ob02276f
UR - https://doi.org/10.1039/c6ob02276f
TI - Metal-free radical thiolations mediated by very weak bases
T2 - Organic and Biomolecular Chemistry
AU - Koziakov, Denis
AU - Májek, Michal
AU - von Wangelin, A. Jacobi
PY - 2016
DA - 2016/11/24
PB - Royal Society of Chemistry (RSC)
SP - 11347-11352
IS - 48
VL - 14
PMID - 27883150
SN - 1477-0520
SN - 1477-0539
ER -
Cite this
BibTex (up to 50 authors)
Copy
@article{2016_Koziakov,
author = {Denis Koziakov and Michal Májek and A. Jacobi von Wangelin},
title = {Metal-free radical thiolations mediated by very weak bases},
journal = {Organic and Biomolecular Chemistry},
year = {2016},
volume = {14},
publisher = {Royal Society of Chemistry (RSC)},
month = {nov},
url = {https://doi.org/10.1039/c6ob02276f},
number = {48},
pages = {11347--11352},
doi = {10.1039/c6ob02276f}
}
Cite this
MLA
Copy
Koziakov, Denis, et al. “Metal-free radical thiolations mediated by very weak bases.” Organic and Biomolecular Chemistry, vol. 14, no. 48, Nov. 2016, pp. 11347-11352. https://doi.org/10.1039/c6ob02276f.
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