Open Access
Open access
volume 11 issue 51 pages 32227-32235

Sample preparation considerations for surface and crystalline properties and ecotoxicity of bare and silica-coated magnetite nanoparticles

Vera Terekhova 2
Gulzhian Dzhardimalieva 1, 4
Natalya Tropskaya 1, 6
Publication typeJournal Article
Publication date2021-09-29
scimago Q1
wos Q2
SJR0.777
CiteScore7.6
Impact factor4.6
ISSN20462069
PubMed ID:  35495499
General Chemistry
General Chemical Engineering
Abstract
Magnetite (Fe3O4) nanoparticles (NPs) have widely used in various fields, including in medicine, due to their (super)paramagnetic properties. This requires a thorough evaluation of their possible hazardous effects. However, there is no standard procedure for the preparation of oxidation-prone NPs (such as magnetite) before subjecting them to biological assays. In this study we used Fe3O4 NPs (bare and silica-coated) as test samples to compare different preparation methods (ultrasound, centrifugation and filteration of NPs suspensions) based on X-ray and dynamic light scattering analysis and evaluation of microstructure and surface charge. After oxidation and functionalization, all samples retained their superparamagnetic behaviour. The toxicity of NP suspensions obtained by the methods described for Paramecium caudatum ciliates and Sinapis alba plants was evaluated.
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Bondarenko L. S. et al. Sample preparation considerations for surface and crystalline properties and ecotoxicity of bare and silica-coated magnetite nanoparticles // RSC Advances. 2021. Vol. 11. No. 51. pp. 32227-32235.
GOST all authors (up to 50) Copy
Bondarenko L. S., Terekhova V. A., Terekhova V., Renieri E., Dzhardimalieva G. I., Dzhardimalieva G., Kelbysheva E., Tropskaya N., Kydralieva K. Sample preparation considerations for surface and crystalline properties and ecotoxicity of bare and silica-coated magnetite nanoparticles // RSC Advances. 2021. Vol. 11. No. 51. pp. 32227-32235.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1039/d1ra05703k
UR - https://xlink.rsc.org/?DOI=D1RA05703K
TI - Sample preparation considerations for surface and crystalline properties and ecotoxicity of bare and silica-coated magnetite nanoparticles
T2 - RSC Advances
AU - Bondarenko, Lyubov S
AU - Terekhova, Vera A.
AU - Terekhova, Vera
AU - Renieri, Elisavet
AU - Dzhardimalieva, G I
AU - Dzhardimalieva, Gulzhian
AU - Kelbysheva, Elena
AU - Tropskaya, Natalya
AU - Kydralieva, Kamila
PY - 2021
DA - 2021/09/29
PB - Royal Society of Chemistry (RSC)
SP - 32227-32235
IS - 51
VL - 11
PMID - 35495499
SN - 2046-2069
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2021_Bondarenko,
author = {Lyubov S Bondarenko and Vera A. Terekhova and Vera Terekhova and Elisavet Renieri and G I Dzhardimalieva and Gulzhian Dzhardimalieva and Elena Kelbysheva and Natalya Tropskaya and Kamila Kydralieva},
title = {Sample preparation considerations for surface and crystalline properties and ecotoxicity of bare and silica-coated magnetite nanoparticles},
journal = {RSC Advances},
year = {2021},
volume = {11},
publisher = {Royal Society of Chemistry (RSC)},
month = {sep},
url = {https://xlink.rsc.org/?DOI=D1RA05703K},
number = {51},
pages = {32227--32235},
doi = {10.1039/d1ra05703k}
}
MLA
Cite this
MLA Copy
Bondarenko, Lyubov S., et al. “Sample preparation considerations for surface and crystalline properties and ecotoxicity of bare and silica-coated magnetite nanoparticles.” RSC Advances, vol. 11, no. 51, Sep. 2021, pp. 32227-32235. https://xlink.rsc.org/?DOI=D1RA05703K.