Zirconium complexes incorporating the new tridentate diamide ligand [(Me3Si)N{CH2CH2N(SiMe3)}2]2–(L); the crystal structures of [Zr(BH4)2L] and [ZrCl{CH(SiMe3)2}L]
Publication type: Journal Article
Publication date: 1995-01-01
SJR: —
CiteScore: —
Impact factor: —
ISSN: 14727773, 13645447, 1470479X, 03009246
General Chemistry
Abstract
The lithium complex of the sterically demanding, polyfunctional amide ligand [(Me3Si)N-{CH2CH2N(SiMe3)}2]2–,Li2L reacted with [ZrCl4(thf)2](thf = tetrahydrofuran) to form dimeric [(ZrCl2L)2]2, in which the ligand is facially co-ordinated in a tridentate manner. Treatment of 2 with LiBH4 or Li[CH(SiMe3)2] generated [Zr(H3BH)L]3 and [ZrCl{CH(SiMe3)2}L]4, respectively. Variable-temperature NMR studies on 4 give evidence for restricted rotation of both the alkyl and amino SiMe3 groups. The crystal structures of 3 and 4 have been determined.
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Cloke F. G. N., Hitchcock P. B., Love J. B. Zirconium complexes incorporating the new tridentate diamide ligand [(Me3Si)N{CH2CH2N(SiMe3)}2]2–(L); the crystal structures of [Zr(BH4)2L] and [ZrCl{CH(SiMe3)2}L] // Journal of the Chemical Society Dalton Transactions. 1995. Vol. 1. pp. 25-30.
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Cloke F. G. N., Hitchcock P. B., Love J. B. Zirconium complexes incorporating the new tridentate diamide ligand [(Me3Si)N{CH2CH2N(SiMe3)}2]2–(L); the crystal structures of [Zr(BH4)2L] and [ZrCl{CH(SiMe3)2}L] // Journal of the Chemical Society Dalton Transactions. 1995. Vol. 1. pp. 25-30.
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TY - JOUR
DO - 10.1039/dt9950000025
UR - https://doi.org/10.1039/dt9950000025
TI - Zirconium complexes incorporating the new tridentate diamide ligand [(Me3Si)N{CH2CH2N(SiMe3)}2]2–(L); the crystal structures of [Zr(BH4)2L] and [ZrCl{CH(SiMe3)2}L]
T2 - Journal of the Chemical Society Dalton Transactions
AU - Cloke, F. Geoffrey N.
AU - Hitchcock, Peter B.
AU - Love, Jason B
PY - 1995
DA - 1995/01/01
PB - Royal Society of Chemistry (RSC)
SP - 25-30
IS - 1
SN - 1472-7773
SN - 1364-5447
SN - 1470-479X
SN - 0300-9246
ER -
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@article{1995_Cloke,
author = {F. Geoffrey N. Cloke and Peter B. Hitchcock and Jason B Love},
title = {Zirconium complexes incorporating the new tridentate diamide ligand [(Me3Si)N{CH2CH2N(SiMe3)}2]2–(L); the crystal structures of [Zr(BH4)2L] and [ZrCl{CH(SiMe3)2}L]},
journal = {Journal of the Chemical Society Dalton Transactions},
year = {1995},
publisher = {Royal Society of Chemistry (RSC)},
month = {jan},
url = {https://doi.org/10.1039/dt9950000025},
number = {1},
pages = {25--30},
doi = {10.1039/dt9950000025}
}