Direct Synthesis of Deuterium-Labeled O-, S-, N-Vinyl Derivatives from Calcium Carbide
Maria S Ledovskaya
1
,
Vladimir V Voronin
1
,
Konstantin S Rodygin
1, 2
,
Alexandra V Posvyatenko
2, 3, 4
,
Ksenia S Egorova
2
,
Тип публикации: Journal Article
Дата публикации: 2019-04-30
scimago Q2
wos Q2
БС2
SJR: 0.559
CiteScore: 4.6
Impact factor: 2.3
ISSN: 00397881, 1437210X
Catalysis
Organic Chemistry
Краткое описание
A novel methodology for the preparation of trideuterovinyl derivatives of high purity directly from alcohols, thiols, and NH-compounds was developed. Commercially available calcium carbide and D2O acted as a D2-acetylene source, and DMSO-d 6 was used to complete the formation of the D2C=C(D)–X fragment (X = O, S, N). Polymerization of a selected trideuterovinylated compound showed a very promising potential of these substances in the synthesis of labeled polymeric materials. Biological activity of the synthesized trideuterovinyl derivatives was evaluated and the results indicated a significant increase of cytotoxicity upon deuteration.
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ГОСТ
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Ledovskaya M. S. et al. Direct Synthesis of Deuterium-Labeled O-, S-, N-Vinyl Derivatives from Calcium Carbide // Synthesis. 2019. Vol. 51. No. 15. pp. 3001-3013.
ГОСТ со всеми авторами (до 50)
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Ledovskaya M. S., Voronin V. V., Rodygin K. S., Posvyatenko A. V., Egorova K. S., Ananikov V. P. Direct Synthesis of Deuterium-Labeled O-, S-, N-Vinyl Derivatives from Calcium Carbide // Synthesis. 2019. Vol. 51. No. 15. pp. 3001-3013.
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RIS
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TY - JOUR
DO - 10.1055/s-0037-1611518
UR - https://doi.org/10.1055/s-0037-1611518
TI - Direct Synthesis of Deuterium-Labeled O-, S-, N-Vinyl Derivatives from Calcium Carbide
T2 - Synthesis
AU - Ledovskaya, Maria S
AU - Voronin, Vladimir V
AU - Rodygin, Konstantin S
AU - Posvyatenko, Alexandra V
AU - Egorova, Ksenia S
AU - Ananikov, Valentine P.
PY - 2019
DA - 2019/04/30
PB - Georg Thieme Verlag KG
SP - 3001-3013
IS - 15
VL - 51
SN - 0039-7881
SN - 1437-210X
ER -
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BibTex (до 50 авторов)
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@article{2019_Ledovskaya,
author = {Maria S Ledovskaya and Vladimir V Voronin and Konstantin S Rodygin and Alexandra V Posvyatenko and Ksenia S Egorova and Valentine P. Ananikov},
title = {Direct Synthesis of Deuterium-Labeled O-, S-, N-Vinyl Derivatives from Calcium Carbide},
journal = {Synthesis},
year = {2019},
volume = {51},
publisher = {Georg Thieme Verlag KG},
month = {apr},
url = {https://doi.org/10.1055/s-0037-1611518},
number = {15},
pages = {3001--3013},
doi = {10.1055/s-0037-1611518}
}
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MLA
Скопировать
Ledovskaya, Maria S., et al. “Direct Synthesis of Deuterium-Labeled O-, S-, N-Vinyl Derivatives from Calcium Carbide.” Synthesis, vol. 51, no. 15, Apr. 2019, pp. 3001-3013. https://doi.org/10.1055/s-0037-1611518.