New reactions of Hünig's base with S2 Cl2 : Formation of monocyclic 1,2-dithioles
Publication type: Journal Article
Publication date: 2001-01-01
scimago Q3
wos Q3
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Abstract
Systematic variation of the ratio of Huenig's base 1 to S2Cl2 in their reactions in chloroform shows that, in addition to known tricyclic bisdithiolothiazine thiones 4 and 5, monocyclic dithiole-3-thiones 6 and 7 can be isolated; when the inert base DABCO is added the extent of sulfuration of the products is reduced and thiones are replaced by their oxo analogues, and diisopropylamines 15 are converted into monocyclic dithiol-3-ones 16; an overall mechanistic rationalisation of the results, extending earlier work, is presented.
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Konstantinova L. S. et al. New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles // Mendeleev Communications. 2001. Vol. 11. No. 5. pp. 165-166.
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Konstantinova L. S., Rakitin O. A., Rees C. W. New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles // Mendeleev Communications. 2001. Vol. 11. No. 5. pp. 165-166.
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TY - JOUR
DO - 10.1070/MC2001v011n05ABEH001493
UR - https://linkinghub.elsevier.com/retrieve/pii/S0959943601707705
TI - New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles
T2 - Mendeleev Communications
AU - Konstantinova, Lidia S.
AU - Rakitin, Oleg A.
AU - Rees, Charles W.
PY - 2001
DA - 2001/01/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 165-166
IS - 5
VL - 11
SN - 0959-9436
SN - 1364-551X
ER -
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BibTex (up to 50 authors)
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@article{2001_Konstantinova,
author = {Lidia S. Konstantinova and Oleg A. Rakitin and Charles W. Rees},
title = {New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles},
journal = {Mendeleev Communications},
year = {2001},
volume = {11},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jan},
url = {https://linkinghub.elsevier.com/retrieve/pii/S0959943601707705},
number = {5},
pages = {165--166},
doi = {10.1070/MC2001v011n05ABEH001493}
}
Cite this
MLA
Copy
Konstantinova, Lidia S., et al. “New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles.” Mendeleev Communications, vol. 11, no. 5, Jan. 2001, pp. 165-166. https://linkinghub.elsevier.com/retrieve/pii/S0959943601707705.