Mendeleev Communications

, том 11 , издание 5 , страницы 165-166

New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles

Lidia S. Konstantinova ¹

Oleg A. Rakitin ¹

Charles W. Rees ²

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N.D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 119991,Moscow, Russian Federation |

Department of Chemistry Imperial College of Science, Technology and Medicine, London SW7 2AY, UK |

Тип публикации: Journal Article

Дата публикации: 2001-01-01

OOO Zhurnal "Mendeleevskie Soobshcheniya"

Mendeleev Communications

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SJR: 0.305

CiteScore: 3.0

Impact factor: 1.7

ISSN: 09599436, 1364551X

DOI: 10.1070/MC2001v011n05ABEH001493

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General Chemistry

Краткое описание

Systematic variation of the ratio of Huenig's base 1 to S2Cl2 in their reactions in chloroform shows that, in addition to known tricyclic bisdithiolothiazine thiones 4 and 5, monocyclic dithiole-3-thiones 6 and 7 can be isolated; when the inert base DABCO is added the extent of sulfuration of the products is reduced and thiones are replaced by their oxo analogues, and diisopropylamines 15 are converted into monocyclic dithiol-3-ones 16; an overall mechanistic rationalisation of the results, extending earlier work, is presented.

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Московский государственный университет имени М.В. Ломоносова

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Konstantinova L. S. et al. New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles // Mendeleev Communications. 2001. Vol. 11. No. 5. pp. 165-166.

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Konstantinova L. S., Rakitin O. A., Rees C. W. New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles // Mendeleev Communications. 2001. Vol. 11. No. 5. pp. 165-166.

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TY - JOUR

DO - 10.1070/MC2001v011n05ABEH001493

UR - https://linkinghub.elsevier.com/retrieve/pii/S0959943601707705

TI - New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles

T2 - Mendeleev Communications

AU - Konstantinova, Lidia S.

AU - Rakitin, Oleg A.

AU - Rees, Charles W.

PY - 2001

DA - 2001/01/01

PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"

SP - 165-166

IS - 5

VL - 11

SN - 0959-9436

SN - 1364-551X

ER -

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@article{2001_Konstantinova,

author = {Lidia S. Konstantinova and Oleg A. Rakitin and Charles W. Rees},

title = {New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles},

journal = {Mendeleev Communications},

year = {2001},

volume = {11},

publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},

month = {jan},

url = {https://linkinghub.elsevier.com/retrieve/pii/S0959943601707705},

number = {5},

pages = {165--166},

doi = {10.1070/MC2001v011n05ABEH001493}

}

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Konstantinova, Lidia S., et al. “New reactions of Hünig's base with S2Cl2: Formation of monocyclic 1,2-dithioles.” Mendeleev Communications, vol. 11, no. 5, Jan. 2001, pp. 165-166. https://linkinghub.elsevier.com/retrieve/pii/S0959943601707705.