An Improved Procedure for the Synthesis of Bicyclo[2.2.2]octane- 2,6-dione
2
Centre for Analysis and Synthesis
Publication type: Journal Article
Publication date: 1993-06-01
scimago Q3
wos Q3
SJR: 0.322
CiteScore: 4.3
Impact factor: 1.8
ISSN: 00397911, 15322432
Organic Chemistry
Abstract
Abstract Conjugate addition of Meldrum's acid to 2-cyclohexenone followed by direct cyclization in PPA/acetic acid constitutes a shorter, more reproducible and higher yielding route to bicyclo[2.2.2]octane-2,6-dione than previous methods. The crude dione could be used as substrate for the baker's yeast reduction to (1R, 4S, 6S)-bicyclo[2.2.2]octane-6-ol-2-one.
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GOST
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Almqvist F., Eklund L., Frejd T. An Improved Procedure for the Synthesis of Bicyclo[2.2.2]octane- 2,6-dione // Synthetic Communications. 1993. Vol. 23. No. 11. pp. 1499-1505.
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Almqvist F., Eklund L., Frejd T. An Improved Procedure for the Synthesis of Bicyclo[2.2.2]octane- 2,6-dione // Synthetic Communications. 1993. Vol. 23. No. 11. pp. 1499-1505.
Cite this
RIS
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TY - JOUR
DO - 10.1080/00397919308011243
UR - https://doi.org/10.1080/00397919308011243
TI - An Improved Procedure for the Synthesis of Bicyclo[2.2.2]octane- 2,6-dione
T2 - Synthetic Communications
AU - Almqvist, Fredrik
AU - Eklund, Lars
AU - Frejd, Torbjöm
PY - 1993
DA - 1993/06/01
PB - Taylor & Francis
SP - 1499-1505
IS - 11
VL - 23
SN - 0039-7911
SN - 1532-2432
ER -
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BibTex (up to 50 authors)
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@article{1993_Almqvist,
author = {Fredrik Almqvist and Lars Eklund and Torbjöm Frejd},
title = {An Improved Procedure for the Synthesis of Bicyclo[2.2.2]octane- 2,6-dione},
journal = {Synthetic Communications},
year = {1993},
volume = {23},
publisher = {Taylor & Francis},
month = {jun},
url = {https://doi.org/10.1080/00397919308011243},
number = {11},
pages = {1499--1505},
doi = {10.1080/00397919308011243}
}
Cite this
MLA
Copy
Almqvist, Fredrik, et al. “An Improved Procedure for the Synthesis of Bicyclo[2.2.2]octane- 2,6-dione.” Synthetic Communications, vol. 23, no. 11, Jun. 1993, pp. 1499-1505. https://doi.org/10.1080/00397919308011243.