Magic Angle Spinning
Тип публикации: Journal Article
Дата публикации: 1981-08-01
SCImago Q3
WOS Q2
БС1
SJR: 0.274
CiteScore: 4.5
Impact factor: 0.6
ISSN: 0144235X, 1366591X
Physical and Theoretical Chemistry
Краткое описание
Abstract Rapid specimen rotation about an axis inclined at the magic angle of 54° 44′ to the direction of the applied magnetic field can remove many sources of broadening from the NMR spectrum of a solid and enable finer features to be revealed. The review commences with a discussion of the basic principles of magic angle spinning and an examination of the effects on magnetic dipolar interactions, the chemical shift interaction, pseudo-dipolar interactions and electric quadrupolar interactions. The anisotropic parts of these interactions are removed from the central spectrum and appear as spinning sidebands. The interactions that remain are the isotropic shifts and J couplings as in isotropic fluids; however some essential differences between solids and fluids remain. Examples of the effects of magic angle spinning on a variety of interactions and materials are given. When applied to metals the anisotropy of Knight shift is removed, isotropic Knight shifts may be measured with precision, and the Ruderman-...
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121
Всего цитирований:
121
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MLA
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ГОСТ
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Andrew E. R. Magic Angle Spinning // International Reviews in Physical Chemistry. 1981. Vol. 1. No. 2. pp. 195-224.
ГОСТ со всеми авторами (до 50)
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Andrew E. R. Magic Angle Spinning // International Reviews in Physical Chemistry. 1981. Vol. 1. No. 2. pp. 195-224.
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RIS
Скопировать
TY - JOUR
DO - 10.1080/01442358109353320
UR - https://doi.org/10.1080/01442358109353320
TI - Magic Angle Spinning
T2 - International Reviews in Physical Chemistry
AU - Andrew, E. R.
PY - 1981
DA - 1981/08/01
PB - Taylor & Francis
SP - 195-224
IS - 2
VL - 1
SN - 0144-235X
SN - 1366-591X
ER -
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BibTex (до 50 авторов)
Скопировать
@article{1981_Andrew,
author = {E. R. Andrew},
title = {Magic Angle Spinning},
journal = {International Reviews in Physical Chemistry},
year = {1981},
volume = {1},
publisher = {Taylor & Francis},
month = {aug},
url = {https://doi.org/10.1080/01442358109353320},
number = {2},
pages = {195--224},
doi = {10.1080/01442358109353320}
}
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MLA
Скопировать
Andrew, E. R.. “Magic Angle Spinning.” International Reviews in Physical Chemistry, vol. 1, no. 2, Aug. 1981, pp. 195-224. https://doi.org/10.1080/01442358109353320.
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