Crystallography Reports

, том 49 , издание 6 , страницы 982-989

Crystal structure and vibrational spectra of N,N′-Di(2,4- dinitrophenyl)diaza-18-Crown-6 and N,N′-Di(tetrafluoropyridyl)diaza-18- Crown-6

L Kh Minacheva ¹

I. S. Ivanova ¹

E N Pyatova ¹

V S Sergienko ¹

G.A Artamkina ²

I P Beletskaya ²

A. Yu. Tsivadze ¹

Скрыть аффилиации авторов Показать аффилиации авторов: 2 аффилиации

Kurnakov institute of General and Inorganic Chemistry, Russian Academy of Sciences, Moscow, Russia |

Moscow State University, Vorob’evy Gory, Moscow, Russia |

Тип публикации: Journal Article

Дата публикации: 2004-11-01

Pleiades Publishing

Crystallography Reports

scimago Q4

wos Q4

БС2

SJR: 0.145

CiteScore: 0.8

Impact factor: 0.5

ISSN: 10637745, 1562689X

DOI: 10.1134/1.1828143

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General Chemistry

Condensed Matter Physics

General Materials Science

Краткое описание

Two new diaza-18-crown-6 derivatives, namely, N,N′-di(2,4-dinitrophenyl)diaza-18-crown-6 (I) and N,N′-di(tetrafluoropyridyl)diaza-18-crown-6 (II), are studied using X-ray diffraction. The vibrational spectra of these compounds are measured and analyzed. Crystals I are monoclinic, a = 9.746(2) Å, b = 12.117(4) Å, c = 11.378(6) Å, β = 98.90(3)°, V = 1327.5(4) Å3, Z = 2, space group P21/c, and R = 0.055 for 1013 reflections with I > 2σ(I). Crystals II are orthorhombic, a = 8.225(4) Å, b = 11.816(4) Å, c = 24.626(5) Å, V = 2393.3(9) Å 3, Z = 4, space group Pbca, and R = 0.035 for 451 reflections with I > 2σ(I). Molecules I and II have a centrosymmetric structure and different conformations. It is demonstrated that the shape and size of the cavity and the conformation of the macrocycle depend substantially on the structure of the substituents at the nitrogen atoms of diaza-18-crown-6.

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Journal of the Iranian Chemical Society	Journal of the Iranian Chemical Society, 1, 50% Journal of the Iranian Chemical Society 1 публикация, 50%
New Journal of Chemistry	New Journal of Chemistry, 1, 50% New Journal of Chemistry 1 публикация, 50%
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Springer Nature	Springer Nature, 1, 50% Springer Nature 1 публикация, 50%
Royal Society of Chemistry (RSC)	Royal Society of Chemistry (RSC), 1, 50% Royal Society of Chemistry (RSC) 1 публикация, 50%
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Minacheva L. Kh. et al. Crystal structure and vibrational spectra of N,N′-Di(2,4- dinitrophenyl)diaza-18-Crown-6 and N,N′-Di(tetrafluoropyridyl)diaza-18- Crown-6 // Crystallography Reports. 2004. Vol. 49. No. 6. pp. 982-989.

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Minacheva L. Kh., Ivanova I. S., Pyatova E. N., Sergienko V. S., Artamkina G., Beletskaya I. P., Tsivadze A. Y. Crystal structure and vibrational spectra of N,N′-Di(2,4- dinitrophenyl)diaza-18-Crown-6 and N,N′-Di(tetrafluoropyridyl)diaza-18- Crown-6 // Crystallography Reports. 2004. Vol. 49. No. 6. pp. 982-989.

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TY - JOUR

DO - 10.1134/1.1828143

UR - https://link.springer.com/10.1134/1.1828143

TI - Crystal structure and vibrational spectra of N,N′-Di(2,4- dinitrophenyl)diaza-18-Crown-6 and N,N′-Di(tetrafluoropyridyl)diaza-18- Crown-6

T2 - Crystallography Reports

AU - Minacheva, L Kh

AU - Ivanova, I. S.

AU - Pyatova, E N

AU - Sergienko, V S

AU - Artamkina, G.A

AU - Beletskaya, I P

AU - Tsivadze, A. Yu.

PY - 2004

DA - 2004/11/01

PB - Pleiades Publishing

SP - 982-989

IS - 6

VL - 49

SN - 1063-7745

SN - 1562-689X

ER -

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@article{2004_Minacheva,

author = {L Kh Minacheva and I. S. Ivanova and E N Pyatova and V S Sergienko and G.A Artamkina and I P Beletskaya and A. Yu. Tsivadze},

title = {Crystal structure and vibrational spectra of N,N′-Di(2,4- dinitrophenyl)diaza-18-Crown-6 and N,N′-Di(tetrafluoropyridyl)diaza-18- Crown-6},

journal = {Crystallography Reports},

year = {2004},

volume = {49},

publisher = {Pleiades Publishing},

month = {nov},

url = {https://link.springer.com/10.1134/1.1828143},

number = {6},

pages = {982--989},

doi = {10.1134/1.1828143}

}

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Minacheva, L. Kh., et al. “Crystal structure and vibrational spectra of N,N′-Di(2,4- dinitrophenyl)diaza-18-Crown-6 and N,N′-Di(tetrafluoropyridyl)diaza-18- Crown-6.” Crystallography Reports, vol. 49, no. 6, Nov. 2004, pp. 982-989. https://link.springer.com/10.1134/1.1828143.