Palladium acetate complexes with morpholine and 4-methylmorpholine. the structure of Pd(C4 H9 ON)2 (OAc)2 • 2H2 O
Тип публикации: Journal Article
Дата публикации: 2006-04-10
scimago Q3
wos Q4
БС2
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Краткое описание
Methods for the synthesis of new palladium(II) acetate complexes [L2Pd(OCOCH3)2], where L is N-coordinated morpholine (C4H9ON) or 4-methylmorpholine (C5H11ON), have been developed. The structure of the complex (C4H9ON)2Pd(OAc)2 · 2H2O (1) has been established by X-ray diffraction. The crystals of 1 are monoclinic (C12H26O8N2Pd, M = 434.76), space group P2(1)/c, a = 9.129(3) Å, b = 16.227(5) Å, c = 6.159(2) Å, V = 878.5(5) Å3, Z = 2. The palladium atom has a square-planar environment with the trans arrangement of ligands. The complex (C5H11ON)2Pd(OAc)2 (2) has a similar structure, according to spectroscopic data.
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Shishilov O. N. et al. Palladium acetate complexes with morpholine and 4-methylmorpholine. the structure of Pd(C4H9ON)2(OAc)2 • 2H2O // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 4. pp. 574-580.
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Shishilov O. N., Stromnova T. A., Churakov A., Kuz'mina L. G., Efimenko I. A. Palladium acetate complexes with morpholine and 4-methylmorpholine. the structure of Pd(C4H9ON)2(OAc)2 • 2H2O // Russian Journal of Inorganic Chemistry. 2006. Vol. 51. No. 4. pp. 574-580.
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TY - JOUR
DO - 10.1134/S0036023606040127
UR - http://link.springer.com/10.1134/S0036023606040127
TI - Palladium acetate complexes with morpholine and 4-methylmorpholine. the structure of Pd(C4H9ON)2(OAc)2 • 2H2O
T2 - Russian Journal of Inorganic Chemistry
AU - Shishilov, O N
AU - Stromnova, T. A.
AU - Churakov, A.V.
AU - Kuz'mina, L. G.
AU - Efimenko, I A
PY - 2006
DA - 2006/04/10
PB - Pleiades Publishing
SP - 574-580
IS - 4
VL - 51
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2006_Shishilov,
author = {O N Shishilov and T. A. Stromnova and A.V. Churakov and L. G. Kuz'mina and I A Efimenko},
title = {Palladium acetate complexes with morpholine and 4-methylmorpholine. the structure of Pd(C4H9ON)2(OAc)2 • 2H2O},
journal = {Russian Journal of Inorganic Chemistry},
year = {2006},
volume = {51},
publisher = {Pleiades Publishing},
month = {apr},
url = {http://link.springer.com/10.1134/S0036023606040127},
number = {4},
pages = {574--580},
doi = {10.1134/S0036023606040127}
}
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MLA
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Shishilov, O. N., et al. “Palladium acetate complexes with morpholine and 4-methylmorpholine. the structure of Pd(C4H9ON)2(OAc)2 • 2H2O.” Russian Journal of Inorganic Chemistry, vol. 51, no. 4, Apr. 2006, pp. 574-580. http://link.springer.com/10.1134/S0036023606040127.