volume 55 issue 11 pages 1754-1761

Thermal behavior of samarium binuclear pivalate and tris-pivalate

A L Emelina 1
Zh V Dobrokhotova 2
A A Sinelshchikova 1
Yu.A. Velikodnyi 1
I.G. Fomina 2
P S Koroteev 2
V. M. Novotortsev 2
Publication typeJournal Article
Publication date2010-11-03
scimago Q3
wos Q4
SJR0.270
CiteScore3.0
Impact factor1.5
ISSN00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Abstract
Kinetic analysis of the thermolysis of samarium pivalate [Sm2(μ2-OOCCMe3)4(OOCCMe3)2(HOOCCMe3)6] · HOOCCMe3 (1) was carried out (the input data were differential scanning calorimetry (DSC) and thermogravimetry data), and a mathematic model of the process was developed that allowed us to optimize (by calculation) the conditions for formation of {Sm(OOCCMe3)3}n (2) samarium tris-pivalate via thermal decomposition of complex 1. The results of the thermal study of samarium and gadolinium tris-pivalates in the temperature range of −50…+50°C are reported. Specific anomalies were found in the DSC curves and heat capacity versus temperature curves in the temperature range of 0–50°C.
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Emelina A. L. et al. Thermal behavior of samarium binuclear pivalate and tris-pivalate // Russian Journal of Inorganic Chemistry. 2010. Vol. 55. No. 11. pp. 1754-1761.
GOST all authors (up to 50) Copy
Emelina A. L., Dobrokhotova Z. V., Sinelshchikova A. A., Velikodnyi Y., Fomina I., Koroteev P. S., Novotortsev V. M., Eremenko I. L. Thermal behavior of samarium binuclear pivalate and tris-pivalate // Russian Journal of Inorganic Chemistry. 2010. Vol. 55. No. 11. pp. 1754-1761.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1134/S0036023610110124
UR - https://doi.org/10.1134/S0036023610110124
TI - Thermal behavior of samarium binuclear pivalate and tris-pivalate
T2 - Russian Journal of Inorganic Chemistry
AU - Emelina, A L
AU - Dobrokhotova, Zh V
AU - Sinelshchikova, A A
AU - Velikodnyi, Yu.A.
AU - Fomina, I.G.
AU - Koroteev, P S
AU - Novotortsev, V. M.
AU - Eremenko, I. L.
PY - 2010
DA - 2010/11/03
PB - Pleiades Publishing
SP - 1754-1761
IS - 11
VL - 55
SN - 0036-0236
SN - 1531-8613
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2010_Emelina,
author = {A L Emelina and Zh V Dobrokhotova and A A Sinelshchikova and Yu.A. Velikodnyi and I.G. Fomina and P S Koroteev and V. M. Novotortsev and I. L. Eremenko},
title = {Thermal behavior of samarium binuclear pivalate and tris-pivalate},
journal = {Russian Journal of Inorganic Chemistry},
year = {2010},
volume = {55},
publisher = {Pleiades Publishing},
month = {nov},
url = {https://doi.org/10.1134/S0036023610110124},
number = {11},
pages = {1754--1761},
doi = {10.1134/S0036023610110124}
}
MLA
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MLA Copy
Emelina, A. L., et al. “Thermal behavior of samarium binuclear pivalate and tris-pivalate.” Russian Journal of Inorganic Chemistry, vol. 55, no. 11, Nov. 2010, pp. 1754-1761. https://doi.org/10.1134/S0036023610110124.