Synthesis, vibrational spectra, and crystal and molecular structure of copper 1,5-Bis[2-(dihydroxyphosphinyl)phenoxy]-3-oxapentane dihydrate [Cu(H 2 L2)(H2 O)2 ]
Тип публикации: Journal Article
Дата публикации: 2012-05-21
scimago Q3
wos Q4
БС2
SJR: 0.270
CiteScore: 3.0
Impact factor: 1.5
ISSN: 00360236, 15318613
Inorganic Chemistry
Physical and Theoretical Chemistry
Materials Science (miscellaneous)
Краткое описание
A new complex Cu(H2L2)(H2O)2] (I), where H4L2 is 1,5-bis[2-(dihydroxyphosphinyl)phenoxy]-3-oxapentane, has been synthesized and characterized. Its molecular and crystal structure has been determined by X-ray crystallography and vibrational spectroscopy. In mononuclear complex I, the copper(II) cation is in a distorted square-planar environment of two water oxygen atoms and two oxygen atoms of the chelating dianion (H2L2)2−. The crystals are orthorhombic, space group Cmc21, a = 25.909(5) Å, b = 9.1500(18) Å, c = 8.5600(17) Å, V = 2029.3(7) Å3, Z = 4, ρcalc = 1.688 g cm−3, μ = 1.292 cm−1; 3107 measured reflections, 1174 reflections with I > 2.0σ(I), Rint = 0.0600, GOOF = 1.413, R1 (I > 2σ(I)) = 0.0812, wR2 (I > 2σ(I)) = 0.2145.
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Russian Journal of Inorganic Chemistry
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Baulin B. E. et al. Synthesis, vibrational spectra, and crystal and molecular structure of copper 1,5-Bis[2-(dihydroxyphosphinyl)phenoxy]-3-oxapentane dihydrate [Cu(H 2L2)(H2O)2] // Russian Journal of Inorganic Chemistry. 2012. Vol. 57. No. 5. pp. 671-675.
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Baulin B. E., Kiskin M. A., Ivanova I. S., Pyatova E. N., Baulin D. V., Tsivadze A. Y. Synthesis, vibrational spectra, and crystal and molecular structure of copper 1,5-Bis[2-(dihydroxyphosphinyl)phenoxy]-3-oxapentane dihydrate [Cu(H 2L2)(H2O)2] // Russian Journal of Inorganic Chemistry. 2012. Vol. 57. No. 5. pp. 671-675.
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TY - JOUR
DO - 10.1134/S0036023612050038
UR - http://link.springer.com/10.1134/S0036023612050038
TI - Synthesis, vibrational spectra, and crystal and molecular structure of copper 1,5-Bis[2-(dihydroxyphosphinyl)phenoxy]-3-oxapentane dihydrate [Cu(H 2L2)(H2O)2]
T2 - Russian Journal of Inorganic Chemistry
AU - Baulin, B E
AU - Kiskin, M. A.
AU - Ivanova, I. S.
AU - Pyatova, E N
AU - Baulin, D V
AU - Tsivadze, A. Yu.
PY - 2012
DA - 2012/05/21
PB - Pleiades Publishing
SP - 671-675
IS - 5
VL - 57
SN - 0036-0236
SN - 1531-8613
ER -
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@article{2012_Baulin,
author = {B E Baulin and M. A. Kiskin and I. S. Ivanova and E N Pyatova and D V Baulin and A. Yu. Tsivadze},
title = {Synthesis, vibrational spectra, and crystal and molecular structure of copper 1,5-Bis[2-(dihydroxyphosphinyl)phenoxy]-3-oxapentane dihydrate [Cu(H 2L2)(H2O)2]},
journal = {Russian Journal of Inorganic Chemistry},
year = {2012},
volume = {57},
publisher = {Pleiades Publishing},
month = {may},
url = {http://link.springer.com/10.1134/S0036023612050038},
number = {5},
pages = {671--675},
doi = {10.1134/S0036023612050038}
}
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Baulin, B. E., et al. “Synthesis, vibrational spectra, and crystal and molecular structure of copper 1,5-Bis[2-(dihydroxyphosphinyl)phenoxy]-3-oxapentane dihydrate [Cu(H 2L2)(H2O)2].” Russian Journal of Inorganic Chemistry, vol. 57, no. 5, May. 2012, pp. 671-675. http://link.springer.com/10.1134/S0036023612050038.
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