Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination
Publication type: Journal Article
Publication date: 2013-09-15
scimago Q3
wos Q4
SJR: 0.252
CiteScore: 1.9
Impact factor: 1.1
ISSN: 10619348, 16083199
Analytical Chemistry
Abstract
We studied the adsorption of sulfanilamide, sulfamethazine, sulfamethoxazole, sulfamethoxypyridazine, and sulfachloropyridazine on hypercrosslinked polystyrene, polymer adsorbents Strata-X and Strata SDB-L, carbon nanomaterial Taunit, and Diasorb-100-C16T depending on the acidity of the solution and the concentration of adsorbates. Conditions were optimized for the preconcentration of sulfanilamides on a microcolumn packed with hypercrosslinked polystyrene. The compounds were desorbed with 1 mL of acetonitrile and determined in the eluate by reversed-phase HPLC with spectrophotometric detection at 255 nm. The preconcentration step decreases the detection limits for sulfanilamides by more than 60 times (to 3 ng/mL). The procedure was used for the analysis of a model mixture in river water.
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Total citations:
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Citations from 2024:
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(11%)
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Dmitrienko S. G. et al. Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination // Journal of Analytical Chemistry. 2013. Vol. 68. No. 10. pp. 871-879.
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Dmitrienko S. G., Kochuk E. V., Tolmacheva V., Apyari V. V., Zolotov Y. Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination // Journal of Analytical Chemistry. 2013. Vol. 68. No. 10. pp. 871-879.
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TY - JOUR
DO - 10.1134/S1061934813100055
UR - http://link.springer.com/10.1134/S1061934813100055
TI - Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination
T2 - Journal of Analytical Chemistry
AU - Dmitrienko, S G
AU - Kochuk, E V
AU - Tolmacheva, V.V.
AU - Apyari, V V
AU - Zolotov, Yu.A
PY - 2013
DA - 2013/09/15
PB - Pleiades Publishing
SP - 871-879
IS - 10
VL - 68
SN - 1061-9348
SN - 1608-3199
ER -
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BibTex (up to 50 authors)
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@article{2013_Dmitrienko,
author = {S G Dmitrienko and E V Kochuk and V.V. Tolmacheva and V V Apyari and Yu.A Zolotov},
title = {Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination},
journal = {Journal of Analytical Chemistry},
year = {2013},
volume = {68},
publisher = {Pleiades Publishing},
month = {sep},
url = {http://link.springer.com/10.1134/S1061934813100055},
number = {10},
pages = {871--879},
doi = {10.1134/S1061934813100055}
}
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MLA
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Dmitrienko, S. G., et al. “Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination.” Journal of Analytical Chemistry, vol. 68, no. 10, Sep. 2013, pp. 871-879. http://link.springer.com/10.1134/S1061934813100055.