том 68 издание 10 страницы 871-879

Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination

Тип публикацииJournal Article
Дата публикации2013-09-15
scimago Q3
wos Q4
БС3
SJR0.252
CiteScore1.9
Impact factor1.1
ISSN10619348, 16083199
Analytical Chemistry
Краткое описание
We studied the adsorption of sulfanilamide, sulfamethazine, sulfamethoxazole, sulfamethoxypyridazine, and sulfachloropyridazine on hypercrosslinked polystyrene, polymer adsorbents Strata-X and Strata SDB-L, carbon nanomaterial Taunit, and Diasorb-100-C16T depending on the acidity of the solution and the concentration of adsorbates. Conditions were optimized for the preconcentration of sulfanilamides on a microcolumn packed with hypercrosslinked polystyrene. The compounds were desorbed with 1 mL of acetonitrile and determined in the eluate by reversed-phase HPLC with spectrophotometric detection at 255 nm. The preconcentration step decreases the detection limits for sulfanilamides by more than 60 times (to 3 ng/mL). The procedure was used for the analysis of a model mixture in river water.
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Journal of Analytical Chemistry
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Pleiades Publishing
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Dmitrienko S. G. et al. Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination // Journal of Analytical Chemistry. 2013. Vol. 68. No. 10. pp. 871-879.
ГОСТ со всеми авторами (до 50) Скопировать
Dmitrienko S. G., Kochuk E. V., Tolmacheva V., Apyari V. V., Zolotov Y. Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination // Journal of Analytical Chemistry. 2013. Vol. 68. No. 10. pp. 871-879.
RIS |
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TY - JOUR
DO - 10.1134/S1061934813100055
UR - http://link.springer.com/10.1134/S1061934813100055
TI - Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination
T2 - Journal of Analytical Chemistry
AU - Dmitrienko, S G
AU - Kochuk, E V
AU - Tolmacheva, V.V.
AU - Apyari, V V
AU - Zolotov, Yu.A
PY - 2013
DA - 2013/09/15
PB - Pleiades Publishing
SP - 871-879
IS - 10
VL - 68
SN - 1061-9348
SN - 1608-3199
ER -
BibTex |
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@article{2013_Dmitrienko,
author = {S G Dmitrienko and E V Kochuk and V.V. Tolmacheva and V V Apyari and Yu.A Zolotov},
title = {Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination},
journal = {Journal of Analytical Chemistry},
year = {2013},
volume = {68},
publisher = {Pleiades Publishing},
month = {sep},
url = {http://link.springer.com/10.1134/S1061934813100055},
number = {10},
pages = {871--879},
doi = {10.1134/S1061934813100055}
}
MLA
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Dmitrienko, S. G., et al. “Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination.” Journal of Analytical Chemistry, vol. 68, no. 10, Sep. 2013, pp. 871-879. http://link.springer.com/10.1134/S1061934813100055.