Journal of Analytical Chemistry, volume 68, issue 10, pages 871-879

Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination

Publication typeJournal Article
Publication date2013-09-15
Quartile SCImago
Q4
Quartile WOS
Q4
Impact factor1.1
ISSN10619348, 16083199
Analytical Chemistry
Abstract
We studied the adsorption of sulfanilamide, sulfamethazine, sulfamethoxazole, sulfamethoxypyridazine, and sulfachloropyridazine on hypercrosslinked polystyrene, polymer adsorbents Strata-X and Strata SDB-L, carbon nanomaterial Taunit, and Diasorb-100-C16T depending on the acidity of the solution and the concentration of adsorbates. Conditions were optimized for the preconcentration of sulfanilamides on a microcolumn packed with hypercrosslinked polystyrene. The compounds were desorbed with 1 mL of acetonitrile and determined in the eluate by reversed-phase HPLC with spectrophotometric detection at 255 nm. The preconcentration step decreases the detection limits for sulfanilamides by more than 60 times (to 3 ng/mL). The procedure was used for the analysis of a model mixture in river water.

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Dmitrienko S. G. et al. Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination // Journal of Analytical Chemistry. 2013. Vol. 68. No. 10. pp. 871-879.
GOST all authors (up to 50) Copy
Dmitrienko S. G., Kochuk E. V., Tolmacheva V., Apyari V. V., Zolotov Y. Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination // Journal of Analytical Chemistry. 2013. Vol. 68. No. 10. pp. 871-879.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1134/S1061934813100055
UR - https://doi.org/10.1134%2FS1061934813100055
TI - Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination
T2 - Journal of Analytical Chemistry
AU - Dmitrienko, S G
AU - Kochuk, E V
AU - Tolmacheva, V.V.
AU - Apyari, V V
AU - Zolotov, Yu.A
PY - 2013
DA - 2013/09/15 00:00:00
PB - Pleiades Publishing
SP - 871-879
IS - 10
VL - 68
SN - 1061-9348
SN - 1608-3199
ER -
BibTex |
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BibTex Copy
@article{2013_Dmitrienko,
author = {S G Dmitrienko and E V Kochuk and V.V. Tolmacheva and V V Apyari and Yu.A Zolotov},
title = {Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination},
journal = {Journal of Analytical Chemistry},
year = {2013},
volume = {68},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://doi.org/10.1134%2FS1061934813100055},
number = {10},
pages = {871--879},
doi = {10.1134/S1061934813100055}
}
MLA
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MLA Copy
Dmitrienko, S. G., et al. “Comparison of adsorbents for the preconcentration of sulfanilamides from aqueous solutions prior to HPLC determination.” Journal of Analytical Chemistry, vol. 68, no. 10, Sep. 2013, pp. 871-879. https://doi.org/10.1134%2FS1061934813100055.
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