Journal of Analytical Chemistry

, том 71 , издание 14 , страницы 1326-1331

Tris(2,6-dimethoxyphenyl)methyl carbenium ion as a charge derivatization agent for the analysis of primary amines by MALDI mass spectrometry

A P Topolyan ¹

D A Strizhevskaya ¹

M S Slyundina ^{2, 3}

M A Belyaeva ¹

O. M. Ivanova ¹

V A Korshun ^{1, 2}

A. V. Ustinov ¹

I V Mikhura ¹

A.A Formanovsky ¹

R S Borisov ^{3, 4}

Скрыть аффилиации авторов Показать аффилиации авторов: 4 аффилиации

Shemyakin–Ovchinnikov Institute of Bioorganic Chemistry, Moscow, Russia |

Gause Institute of New Antibiotics, Moscow, Russia |

Topchiev Institute of petrochemical synthesis, Moscow, Russia |

⁴

Peoples Friendship University of Russia, Moscow, Russia |

Тип публикации: Journal Article

Дата публикации: 2016-12-01

Pleiades Publishing

Journal of Analytical Chemistry

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wos Q4

БС3

SJR: 0.252

CiteScore: 1.9

Impact factor: 1.1

ISSN: 10619348, 16083199

DOI: 10.1134/S106193481614015X

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Analytical Chemistry

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A novel derivatization method for the analysis of primary amines by MALDI mass spectrometry is proposed. Tris(2,6-dimethoxyphenyl) methyl carbenium cation reacts smoothly with primary amines, forming permanently charged adducts with the mass increment +359 Da and absorbance in the UV region. The approach was tested on a number of amines, including biologically active compounds and therapeutic agents.

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Институт нефтехимического синтеза им. А.В. Топчиева РАН

Российский Университет Дружбы Народов

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Topolyan A. P. et al. Tris(2,6-dimethoxyphenyl)methyl carbenium ion as a charge derivatization agent for the analysis of primary amines by MALDI mass spectrometry // Journal of Analytical Chemistry. 2016. Vol. 71. No. 14. pp. 1326-1331.

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Topolyan A. P., Strizhevskaya D. A., Slyundina M. S., Belyaeva M. A., Ivanova O. M., Korshun V. A., Ustinov A. V., Mikhura I. V., Formanovsky A., Borisov R. S. Tris(2,6-dimethoxyphenyl)methyl carbenium ion as a charge derivatization agent for the analysis of primary amines by MALDI mass spectrometry // Journal of Analytical Chemistry. 2016. Vol. 71. No. 14. pp. 1326-1331.

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TY - JOUR

DO - 10.1134/S106193481614015X

UR - https://doi.org/10.1134/S106193481614015X

TI - Tris(2,6-dimethoxyphenyl)methyl carbenium ion as a charge derivatization agent for the analysis of primary amines by MALDI mass spectrometry

T2 - Journal of Analytical Chemistry

AU - Topolyan, A P

AU - Strizhevskaya, D A

AU - Slyundina, M S

AU - Belyaeva, M A

AU - Ivanova, O. M.

AU - Korshun, V A

AU - Ustinov, A. V.

AU - Mikhura, I V

AU - Formanovsky, A.A

AU - Borisov, R S

PY - 2016

DA - 2016/12/01

PB - Pleiades Publishing

SP - 1326-1331

IS - 14

VL - 71

SN - 1061-9348

SN - 1608-3199

ER -

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@article{2016_Topolyan,

author = {A P Topolyan and D A Strizhevskaya and M S Slyundina and M A Belyaeva and O. M. Ivanova and V A Korshun and A. V. Ustinov and I V Mikhura and A.A Formanovsky and R S Borisov},

title = {Tris(2,6-dimethoxyphenyl)methyl carbenium ion as a charge derivatization agent for the analysis of primary amines by MALDI mass spectrometry},

journal = {Journal of Analytical Chemistry},

year = {2016},

volume = {71},

publisher = {Pleiades Publishing},

month = {dec},

url = {https://doi.org/10.1134/S106193481614015X},

number = {14},

pages = {1326--1331},

doi = {10.1134/S106193481614015X}

}

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Topolyan, A. P., et al. “Tris(2,6-dimethoxyphenyl)methyl carbenium ion as a charge derivatization agent for the analysis of primary amines by MALDI mass spectrometry.” Journal of Analytical Chemistry, vol. 71, no. 14, Dec. 2016, pp. 1326-1331. https://doi.org/10.1134/S106193481614015X.