Journal of Analytical Chemistry, volume 76, issue 8, pages 946-959
Using Hypercrosslinked Polystyrene for the Multicomponent Solid-Phase Extraction of Residues of 63 Veterinary Preparations in Their Determination in Chicken Meat by High-Performance Liquid Chromatography–Tandem Mass Spectrometry
Melekhin A O
1, 2
,
Tolmacheva V.V.
1
,
Shubina E G
2
,
Dmitrienko S G
1
,
Apyari V V
1
,
Grudev A I
2
2
Central Scientific and Methodological Veterinary Laboratory, Moscow, Russia
|
Publication type: Journal Article
Publication date: 2021-07-29
Journal:
Journal of Analytical Chemistry
Quartile SCImago
Q4
Quartile WOS
Q4
Impact factor: 1.1
ISSN: 10619348, 16083199
Analytical Chemistry
Abstract
Hypercrosslinked polystyrene is proposed for the multicomponent solid-phase extraction of residues of 63 veterinary preparations from various classes (sulfonamides, tetracyclines, quinolones, amphenicols, nitroimidazoles, β-lactams, macrolides, lincosamides, and pleuromutilins) in their determination in chicken meat by HPLC–tandem mass spectrometry. Sample preparation includes the extraction of analytes with a McIlvaine buffer solution, fat removal by extraction with hexane, and the further purification of the extracts on cartridges with hypercrosslinked polystyrene. The method ensures the quantitative extraction of analytes (recovery rates are from 83 to 117%) and good reproducibility (RSD ≤ 12%). Veterinary preparations were identified by the exact masses of analyte ions formed in electrospray ionization on switching positive and negative polarity. The matrix effect for all veterinary drugs was below 20%. The determination was carried out by the method of matrix calibration; the limits of detection and determination were 0.01–0.3 and 0.02–1 ng/g, respectively. An analysis of contaminated chicken meat samples showed that the results are in satisfactory agreement with the data obtained by the methods adopted in the Russian Federation for the determination of various groups of antibiotics.
Citations by journals
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1
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Food Chemistry
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1 publication, 33.33%
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Molecules
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Journal of Molecular Liquids
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1 publication, 33.33%
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Citations by publishers
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Elsevier
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Elsevier
2 publications, 66.67%
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Multidisciplinary Digital Publishing Institute (MDPI)
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Multidisciplinary Digital Publishing Institute (MDPI)
1 publication, 33.33%
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1
2
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Melekhin A. O. et al. Using Hypercrosslinked Polystyrene for the Multicomponent Solid-Phase Extraction of Residues of 63 Veterinary Preparations in Their Determination in Chicken Meat by High-Performance Liquid Chromatography–Tandem Mass Spectrometry // Journal of Analytical Chemistry. 2021. Vol. 76. No. 8. pp. 946-959.
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Melekhin A. O., Tolmacheva V., Shubina E. G., Dmitrienko S. G., Apyari V. V., Grudev A. I. Using Hypercrosslinked Polystyrene for the Multicomponent Solid-Phase Extraction of Residues of 63 Veterinary Preparations in Their Determination in Chicken Meat by High-Performance Liquid Chromatography–Tandem Mass Spectrometry // Journal of Analytical Chemistry. 2021. Vol. 76. No. 8. pp. 946-959.
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TY - JOUR
DO - 10.1134/S1061934821060046
UR - https://doi.org/10.1134%2FS1061934821060046
TI - Using Hypercrosslinked Polystyrene for the Multicomponent Solid-Phase Extraction of Residues of 63 Veterinary Preparations in Their Determination in Chicken Meat by High-Performance Liquid Chromatography–Tandem Mass Spectrometry
T2 - Journal of Analytical Chemistry
AU - Melekhin, A O
AU - Tolmacheva, V.V.
AU - Dmitrienko, S G
AU - Grudev, A I
AU - Shubina, E G
AU - Apyari, V V
PY - 2021
DA - 2021/07/29 00:00:00
PB - Pleiades Publishing
SP - 946-959
IS - 8
VL - 76
SN - 1061-9348
SN - 1608-3199
ER -
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@article{2021_Melekhin,
author = {A O Melekhin and V.V. Tolmacheva and S G Dmitrienko and A I Grudev and E G Shubina and V V Apyari},
title = {Using Hypercrosslinked Polystyrene for the Multicomponent Solid-Phase Extraction of Residues of 63 Veterinary Preparations in Their Determination in Chicken Meat by High-Performance Liquid Chromatography–Tandem Mass Spectrometry},
journal = {Journal of Analytical Chemistry},
year = {2021},
volume = {76},
publisher = {Pleiades Publishing},
month = {jul},
url = {https://doi.org/10.1134%2FS1061934821060046},
number = {8},
pages = {946--959},
doi = {10.1134/S1061934821060046}
}
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Melekhin, A. O., et al. “Using Hypercrosslinked Polystyrene for the Multicomponent Solid-Phase Extraction of Residues of 63 Veterinary Preparations in Their Determination in Chicken Meat by High-Performance Liquid Chromatography–Tandem Mass Spectrometry.” Journal of Analytical Chemistry, vol. 76, no. 8, Jul. 2021, pp. 946-959. https://doi.org/10.1134%2FS1061934821060046.