,
volume 32
,
issue 3
,
pages 166-172
Zn complex with N-(4′-Benzo-15-crown-5)-2-(amino-N-tosyl)-phenylaldimine: Synthesis, crystal structure, and vibration spectrum
L Kh Minacheva
1
,
I. S. Ivanova
1
,
A V Dorokhov
1
,
A S Burlov
2
,
A. D. Garnovskii
2
,
V S Segienko
1
,
Publication type: Journal Article
Publication date: 2006-03-22
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
The ZnL2 complex (I) (HL = N-(4′-benzo-15-crown-5)-2-(amino-N-tosyl)phenylaldimine) is synthesized and studied by IR spectroscopy and X-ray diffraction analysis. The crystals are monoclinic: a = 23.139(2) Å, b = 19.931(2) Å, c = 14.604(2) Å, β = 121.20(1)°, Z = 4, space group C2/c, R = 0.751 for 766 reflections with I > 2σ(I). The Zn atom in a molecule of the complex lies on a twofold axis and is coordinated at the vertices of a distorted tetrahedron by four N atoms of two HL ligands (average Zn-N distance 2.024 Å).
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Minacheva L. Kh. et al. Zn complex with N-(4′-Benzo-15-crown-5)-2-(amino-N-tosyl)-phenylaldimine: Synthesis, crystal structure, and vibration spectrum // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2006. Vol. 32. No. 3. pp. 166-172.
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Minacheva L. Kh., Ivanova I. S., Dorokhov A. V., Burlov A. S., Garnovskii A. D., Segienko V. S., Tsivadze A. Y. Zn complex with N-(4′-Benzo-15-crown-5)-2-(amino-N-tosyl)-phenylaldimine: Synthesis, crystal structure, and vibration spectrum // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2006. Vol. 32. No. 3. pp. 166-172.
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TY - JOUR
DO - 10.1134/S107032840603002X
UR - http://link.springer.com/10.1134/S107032840603002X
TI - Zn complex with N-(4′-Benzo-15-crown-5)-2-(amino-N-tosyl)-phenylaldimine: Synthesis, crystal structure, and vibration spectrum
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Minacheva, L Kh
AU - Ivanova, I. S.
AU - Dorokhov, A V
AU - Burlov, A S
AU - Garnovskii, A. D.
AU - Segienko, V S
AU - Tsivadze, A. Yu.
PY - 2006
DA - 2006/03/22
PB - Pleiades Publishing
SP - 166-172
IS - 3
VL - 32
SN - 1070-3284
SN - 1608-3318
ER -
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@article{2006_Minacheva,
author = {L Kh Minacheva and I. S. Ivanova and A V Dorokhov and A S Burlov and A. D. Garnovskii and V S Segienko and A. Yu. Tsivadze},
title = {Zn complex with N-(4′-Benzo-15-crown-5)-2-(amino-N-tosyl)-phenylaldimine: Synthesis, crystal structure, and vibration spectrum},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2006},
volume = {32},
publisher = {Pleiades Publishing},
month = {mar},
url = {http://link.springer.com/10.1134/S107032840603002X},
number = {3},
pages = {166--172},
doi = {10.1134/S107032840603002X}
}
Cite this
MLA
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Minacheva, L. Kh., et al. “Zn complex with N-(4′-Benzo-15-crown-5)-2-(amino-N-tosyl)-phenylaldimine: Synthesis, crystal structure, and vibration spectrum.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 32, no. 3, Mar. 2006, pp. 166-172. http://link.springer.com/10.1134/S107032840603002X.
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