,
volume 44
,
issue 8
,
pages 489-495
Synthesis and Spin State of the Cobalt(II) Complexes with Substituted 2,6-Bis(pyrazol-3-yl)pyridine Ligands
A. A. Pavlov
1
,
A. S. Belov
1
,
S A Savkina
1
,
A V Polezhaev
1
,
D Yu Aleshin
2
,
V.V. Novikov
1
,
Yu V Nelyubina
1, 3
Publication type: Journal Article
Publication date: 2018-08-30
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
The direct template reactions afford the cobalt(II) complexes (I–III) with the hydroxy- and acetyl-substituted 2,6-bis(pyrazol-3-yl)pyridine ligands containing the phenyl and 4-tert-butylphenyl group in position 1. All compounds are isolated in the individual state and characterized by elemental analysis and NMR spectroscopy. The X-ray diffraction data obtained for crystals of compound I (СIF file CCDC 1577238) and the data for solutions (using the proposed approach to analysis of paramagnetic NMR shifts on the basis of quantum chemical calculations) show that in the complexes the metal ion exists in the high-spin state (S = 3/2) and undergoes no temperature-induced spin transition in a temperature range of 120–300 K.
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9
Total citations:
9
Citations from 2024:
1
(11.11%)
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4
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Pavlov A. A. et al. Synthesis and Spin State of the Cobalt(II) Complexes with Substituted 2,6-Bis(pyrazol-3-yl)pyridine Ligands // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2018. Vol. 44. No. 8. pp. 489-495.
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Pavlov A. A., Belov A. S., Savkina S. A., Polezhaev A. V., Aleshin D. Yu., Novikov V., Nelyubina Yu. V. Synthesis and Spin State of the Cobalt(II) Complexes with Substituted 2,6-Bis(pyrazol-3-yl)pyridine Ligands // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2018. Vol. 44. No. 8. pp. 489-495.
Cite this
RIS
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TY - JOUR
DO - 10.1134/S1070328418080067
UR - https://doi.org/10.1134/S1070328418080067
TI - Synthesis and Spin State of the Cobalt(II) Complexes with Substituted 2,6-Bis(pyrazol-3-yl)pyridine Ligands
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Pavlov, A. A.
AU - Belov, A. S.
AU - Savkina, S A
AU - Polezhaev, A V
AU - Aleshin, D Yu
AU - Novikov, V.V.
AU - Nelyubina, Yu V
PY - 2018
DA - 2018/08/30
PB - Pleiades Publishing
SP - 489-495
IS - 8
VL - 44
SN - 1070-3284
SN - 1608-3318
ER -
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BibTex (up to 50 authors)
Copy
@article{2018_Pavlov,
author = {A. A. Pavlov and A. S. Belov and S A Savkina and A V Polezhaev and D Yu Aleshin and V.V. Novikov and Yu V Nelyubina},
title = {Synthesis and Spin State of the Cobalt(II) Complexes with Substituted 2,6-Bis(pyrazol-3-yl)pyridine Ligands},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2018},
volume = {44},
publisher = {Pleiades Publishing},
month = {aug},
url = {https://doi.org/10.1134/S1070328418080067},
number = {8},
pages = {489--495},
doi = {10.1134/S1070328418080067}
}
Cite this
MLA
Copy
Pavlov, A. A., et al. “Synthesis and Spin State of the Cobalt(II) Complexes with Substituted 2,6-Bis(pyrazol-3-yl)pyridine Ligands.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 44, no. 8, Aug. 2018, pp. 489-495. https://doi.org/10.1134/S1070328418080067.