,
volume 45
,
issue 4
,
pages 273-287
Atmospheric Oxygen Influence on the Chemical Transformations of 4,5-Dimethyl-1,2-Phenylenediamine in the Reactions with Copper(II) Pivalate
S A Nikolaevskii
1
,
M. A. Kiskin
1
,
A G Starikov
2
,
N. N. Efimov
1
,
A S Bogomyakov
3
,
V V Minin
1
,
E. A. Ugolkova
1
,
O M Nikitin
4
,
T V Magdesieva
4
,
A. A. Sidorov
1
,
1
3
Publication type: Journal Article
Publication date: 2019-04-22
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
The one-pot synthesis of the Cu(II) complex with hard to access symmetric bis-azoligand is carried out by the reaction of 4,5-dimethyl-1,2-phenylenediamine (Dmpda) with the [Cu2(Piv)4(HPiv)2] complex (Piv is the pivalate anion) in the presence of atmospheric oxygen. The amine form of the ligand takes place and the bis-diiminosemiquinone biradical redox form of the ligand does not take place in the [CuLazo] complex as unambiguously shown by the data of X-ray structure analysis (CIF files CCDC nos. 1877582 (I · DMF) and 1877583 (II), ESR spectroscopy, SQUID magnetometry, and electrochemical and quantum chemical studies. The coordination polymer [Cu2(Piv)4(Dmpda)]n in which the Dmpda molecules perform the bridging function is formed in the same reaction mixture under reduced air pressure.
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Nikolaevskii S. A. et al. Atmospheric Oxygen Influence on the Chemical Transformations of 4,5-Dimethyl-1,2-Phenylenediamine in the Reactions with Copper(II) Pivalate // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2019. Vol. 45. No. 4. pp. 273-287.
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Nikolaevskii S. A., Kiskin M. A., Starikov A. G., Efimov N. N., Bogomyakov A. S., Minin V. V., Ugolkova E. A., Nikitin O. M., Magdesieva T. V., Sidorov A. A., Eremenko I. L. Atmospheric Oxygen Influence on the Chemical Transformations of 4,5-Dimethyl-1,2-Phenylenediamine in the Reactions with Copper(II) Pivalate // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2019. Vol. 45. No. 4. pp. 273-287.
Cite this
RIS
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TY - JOUR
DO - 10.1134/S1070328419040067
UR - https://doi.org/10.1134/S1070328419040067
TI - Atmospheric Oxygen Influence on the Chemical Transformations of 4,5-Dimethyl-1,2-Phenylenediamine in the Reactions with Copper(II) Pivalate
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Nikolaevskii, S A
AU - Kiskin, M. A.
AU - Starikov, A G
AU - Efimov, N. N.
AU - Bogomyakov, A S
AU - Minin, V V
AU - Ugolkova, E. A.
AU - Nikitin, O M
AU - Magdesieva, T V
AU - Sidorov, A. A.
AU - Eremenko, I. L.
PY - 2019
DA - 2019/04/22
PB - Pleiades Publishing
SP - 273-287
IS - 4
VL - 45
SN - 1070-3284
SN - 1608-3318
ER -
Cite this
BibTex (up to 50 authors)
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@article{2019_Nikolaevskii,
author = {S A Nikolaevskii and M. A. Kiskin and A G Starikov and N. N. Efimov and A S Bogomyakov and V V Minin and E. A. Ugolkova and O M Nikitin and T V Magdesieva and A. A. Sidorov and I. L. Eremenko},
title = {Atmospheric Oxygen Influence on the Chemical Transformations of 4,5-Dimethyl-1,2-Phenylenediamine in the Reactions with Copper(II) Pivalate},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2019},
volume = {45},
publisher = {Pleiades Publishing},
month = {apr},
url = {https://doi.org/10.1134/S1070328419040067},
number = {4},
pages = {273--287},
doi = {10.1134/S1070328419040067}
}
Cite this
MLA
Copy
Nikolaevskii, S. A., et al. “Atmospheric Oxygen Influence on the Chemical Transformations of 4,5-Dimethyl-1,2-Phenylenediamine in the Reactions with Copper(II) Pivalate.” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 45, no. 4, Apr. 2019, pp. 273-287. https://doi.org/10.1134/S1070328419040067.