Bisisocyanide complexes of Zn(II) halides: Synthesis, structure, and application in the catalysis of isocyanides reaction with secondary amines
Publication type: Journal Article
Publication date: 2017-08-01
scimago Q4
wos Q4
SJR: 0.179
CiteScore: 1.4
Impact factor: 0.8
ISSN: 10703632, 16083350
General Chemistry
Abstract
Isocyanide zinc complexes [ZnX2(CNR)2] (X = Cl, Br, I; R = Xyl, Cy, But) have been prepared via the interaction of the corresponding zinc halides ZnX2 and isocyanide CNR in toluene at 100°C (yield 64–77%) and characterized by the data of elemental analysis, mass spectrometry, IR and NMR spectroscopy, and X-ray diffraction analysis. The zinc complexes [ZnBr2(CNR)2] (R = Xyl, Сy) have been used as catalysts for the synthesis of formamidines R1N=CHNR2 2 [R1 = Xyl, Сy; R2 2 = Et2, (CH2)4, (CH2CH2)2NMe, Me + CH2Ph] from isocyanides CNR1 and secondary amines HNR2 2 in bulk (yield 92–98%).
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Lavnevich L. V. et al. Bisisocyanide complexes of Zn(II) halides: Synthesis, structure, and application in the catalysis of isocyanides reaction with secondary amines // Russian Journal of General Chemistry. 2017. Vol. 87. No. 8. pp. 1752-1758.
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Lavnevich L. V., Avdontseva M. S., Kinzhalov M. A., Bokach N. A. Bisisocyanide complexes of Zn(II) halides: Synthesis, structure, and application in the catalysis of isocyanides reaction with secondary amines // Russian Journal of General Chemistry. 2017. Vol. 87. No. 8. pp. 1752-1758.
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TY - JOUR
DO - 10.1134/S1070363217080199
UR - https://doi.org/10.1134/S1070363217080199
TI - Bisisocyanide complexes of Zn(II) halides: Synthesis, structure, and application in the catalysis of isocyanides reaction with secondary amines
T2 - Russian Journal of General Chemistry
AU - Lavnevich, L V
AU - Avdontseva, M S
AU - Kinzhalov, M A
AU - Bokach, N A
PY - 2017
DA - 2017/08/01
PB - Pleiades Publishing
SP - 1752-1758
IS - 8
VL - 87
SN - 1070-3632
SN - 1608-3350
ER -
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BibTex (up to 50 authors)
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@article{2017_Lavnevich,
author = {L V Lavnevich and M S Avdontseva and M A Kinzhalov and N A Bokach},
title = {Bisisocyanide complexes of Zn(II) halides: Synthesis, structure, and application in the catalysis of isocyanides reaction with secondary amines},
journal = {Russian Journal of General Chemistry},
year = {2017},
volume = {87},
publisher = {Pleiades Publishing},
month = {aug},
url = {https://doi.org/10.1134/S1070363217080199},
number = {8},
pages = {1752--1758},
doi = {10.1134/S1070363217080199}
}
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Lavnevich, L. V., et al. “Bisisocyanide complexes of Zn(II) halides: Synthesis, structure, and application in the catalysis of isocyanides reaction with secondary amines.” Russian Journal of General Chemistry, vol. 87, no. 8, Aug. 2017, pp. 1752-1758. https://doi.org/10.1134/S1070363217080199.
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