Russian Journal of Physical Chemistry B, volume 15, issue 8, pages 1251-1254
Kinetics of Release of a Bifunctional 2,2,5,5-Tetramethyl-4-Phenyl-3-Imidazoline-1-Oxyl-3-Oxide Probe from Poly-D,L-Lactide Films Formed Using Supercritical Carbon Dioxide
Publication type: Journal Article
Publication date: 2021-12-01
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ISSN: 19907931, 19907923
Physical and Theoretical Chemistry
Abstract
Optical spectroscopy and ESR spectroscopy were used for the first time to quantitatively describe the release of a nitroxyl probe from poly-D,L-lactide (PDLLA) films into phosphate buffer. The bifunctional probe, 2,2,5,5-tetramethyl-4-phenyl-3-imidazoline-1-oxyl-3-oxide (IMNO), contains a paramagnetic nitroxyl group and has a high extinction coefficient in the UV spectrum. Polymer films were obtained from porous PDLLA-based matrices formed and doped with IMNO in supercritical CO2 (SC-CO2). The combined use of the above-mentioned methods was shown to be promising to gain a more detailed information on the release of probes from PDLLA films, the duration of which did not exceed three weeks.
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Ivanova T. et al. Kinetics of Release of a Bifunctional 2,2,5,5-Tetramethyl-4-Phenyl-3-Imidazoline-1-Oxyl-3-Oxide Probe from Poly-D,L-Lactide Films Formed Using Supercritical Carbon Dioxide // Russian Journal of Physical Chemistry B. 2021. Vol. 15. No. 8. pp. 1251-1254.
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Ivanova T., Chumakova N. A., Golubeva E. N., Melnikov M. Ya. Kinetics of Release of a Bifunctional 2,2,5,5-Tetramethyl-4-Phenyl-3-Imidazoline-1-Oxyl-3-Oxide Probe from Poly-D,L-Lactide Films Formed Using Supercritical Carbon Dioxide // Russian Journal of Physical Chemistry B. 2021. Vol. 15. No. 8. pp. 1251-1254.
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TY - JOUR
DO - 10.1134/S1990793121080066
UR - https://doi.org/10.1134%2FS1990793121080066
TI - Kinetics of Release of a Bifunctional 2,2,5,5-Tetramethyl-4-Phenyl-3-Imidazoline-1-Oxyl-3-Oxide Probe from Poly-D,L-Lactide Films Formed Using Supercritical Carbon Dioxide
T2 - Russian Journal of Physical Chemistry B
AU - Ivanova, T.A.
AU - Chumakova, N A
AU - Melnikov, M Ya
AU - Golubeva, E. N.
PY - 2021
DA - 2021/12/01 00:00:00
PB - Pleiades Publishing
SP - 1251-1254
IS - 8
VL - 15
SN - 1990-7931
SN - 1990-7923
ER -
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@article{2021_Ivanova,
author = {T.A. Ivanova and N A Chumakova and M Ya Melnikov and E. N. Golubeva},
title = {Kinetics of Release of a Bifunctional 2,2,5,5-Tetramethyl-4-Phenyl-3-Imidazoline-1-Oxyl-3-Oxide Probe from Poly-D,L-Lactide Films Formed Using Supercritical Carbon Dioxide},
journal = {Russian Journal of Physical Chemistry B},
year = {2021},
volume = {15},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1134%2FS1990793121080066},
number = {8},
pages = {1251--1254},
doi = {10.1134/S1990793121080066}
}
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Ivanova, T.A., et al. “Kinetics of Release of a Bifunctional 2,2,5,5-Tetramethyl-4-Phenyl-3-Imidazoline-1-Oxyl-3-Oxide Probe from Poly-D,L-Lactide Films Formed Using Supercritical Carbon Dioxide.” Russian Journal of Physical Chemistry B, vol. 15, no. 8, Dec. 2021, pp. 1251-1254. https://doi.org/10.1134%2FS1990793121080066.