Synthesis and molecular structure of bis(benzo)aza-14-crown-4 ethers with 7-azabicyclo[3.3.1]nonane and homologous fragments
A N Levov
1
,
A I Komarov
2
,
A T Soldatenkov
1
,
G V Avramenko
2
,
S A Soldatova
1
,
V. N. Khrustalev
3
Publication type: Journal Article
Publication date: 2008-11-01
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Abstract
By condensation of cycloalkanes with 2-{2-[2-(2-formylphenoxy)ethoxy]ethoxy}benzaldehyde and ammonium acetate by Petrenko-Kritchenko method first representatives of new heterocyclic systems, bis(benzo)-aza-14-crown-4 ethers containing a 7-aza-bicyclo[3.3.1]nonane or its homologous fragment, were obtained in 6–15% yield. With growing cycle of the initial cycloketone the yield of the azacrownophane considerably grew. By means of XRD analysis the molecular structure was established of four synthesized macrocycles, the relative configuration of asymmetrical atoms was determined, and the size of the internal cavities of the azacrown part was estimated.
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GOST
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Levov A. N. et al. Synthesis and molecular structure of bis(benzo)aza-14-crown-4 ethers with 7-azabicyclo[3.3.1]nonane and homologous fragments // Russian Journal of Organic Chemistry. 2008. Vol. 44. No. 11. pp. 1665-1670.
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Levov A. N., Komarov A. I., Soldatenkov A. T., Avramenko G. V., Soldatova S. A., Khrustalev V. N. Synthesis and molecular structure of bis(benzo)aza-14-crown-4 ethers with 7-azabicyclo[3.3.1]nonane and homologous fragments // Russian Journal of Organic Chemistry. 2008. Vol. 44. No. 11. pp. 1665-1670.
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RIS
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TY - JOUR
DO - 10.1134/s1070428008110183
UR - https://doi.org/10.1134/s1070428008110183
TI - Synthesis and molecular structure of bis(benzo)aza-14-crown-4 ethers with 7-azabicyclo[3.3.1]nonane and homologous fragments
T2 - Russian Journal of Organic Chemistry
AU - Levov, A N
AU - Komarov, A I
AU - Soldatenkov, A T
AU - Avramenko, G V
AU - Soldatova, S A
AU - Khrustalev, V. N.
PY - 2008
DA - 2008/11/01
PB - Pleiades Publishing
SP - 1665-1670
IS - 11
VL - 44
SN - 1070-4280
SN - 1608-3393
ER -
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BibTex (up to 50 authors)
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@article{2008_Levov,
author = {A N Levov and A I Komarov and A T Soldatenkov and G V Avramenko and S A Soldatova and V. N. Khrustalev},
title = {Synthesis and molecular structure of bis(benzo)aza-14-crown-4 ethers with 7-azabicyclo[3.3.1]nonane and homologous fragments},
journal = {Russian Journal of Organic Chemistry},
year = {2008},
volume = {44},
publisher = {Pleiades Publishing},
month = {nov},
url = {https://doi.org/10.1134/s1070428008110183},
number = {11},
pages = {1665--1670},
doi = {10.1134/s1070428008110183}
}
Cite this
MLA
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Levov, A. N., et al. “Synthesis and molecular structure of bis(benzo)aza-14-crown-4 ethers with 7-azabicyclo[3.3.1]nonane and homologous fragments.” Russian Journal of Organic Chemistry, vol. 44, no. 11, Nov. 2008, pp. 1665-1670. https://doi.org/10.1134/s1070428008110183.