Pleiades Publishing
Russian Journal of Organic Chemistry
,  volume 55 ,  issue 1 ,  pages 101-107

New Tetracyclic Spiro-1,2,4-trioxolanes (Ozonides). Synthesis and Mass Spectrometric Study

Publication type: Journal Article
Publication date: 2019-01-01
Pleiades Publishing
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Abstract
New tetracyclic dispiro-1,2,4-trioxolanes (ozonides) were synthesized by reactions of 5–7-membered alicyclic 1,5-diketones with 30% hydrogen peroxide in diethyl ether or ethanol in the presence of boron trifluoride-diethyl ether complex or a strong mineral acid (HCl, H2SO4, HClO4). Mass spectrometric study of the title compounds under atmospheric pressure chemical ionization revealed specificity of fragment ion decomposition with respect to the ring size, which makes it possible to identify such compounds by their mass spectra.
Found 
Found 
4 citations
Yaremenko Ivan
PhD in Chemistry
60 publications,  1 567 citations,  5 reviews
h-index: 24
N.D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
N.D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
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N.D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
N.D. Zelinsky Institute of Organic Chemistry of the Russian Academy of Sciences
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h-index: 19
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h-index: 29
Lomonosov Moscow State University
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Lomonosov Moscow State University
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A.N. Frumkin Institute of Physical Chemistry and Electrochemistry of the Russian Academy of Sciences
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h-index: 14
Saint Petersburg State University
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A.N.Nesmeyanov Institute of Organoelement Compounds of the Russian Academy of Sciences
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A.E. Arbuzov Institute of Organic and Physical Chemistry of the Kazan Scientific Center of the Russian Academy of Sciences
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North Caucasus Federal University
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Kuban State University
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Biological activity
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Malononitrile
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Asymmetric metal complex catalysis
Chemistry of organic and organoelement compounds; chemistry of polymers; production of materials
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Mendeleev University of Chemical Technology of Russia
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Ural Federal University
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GOST Copy
Akimova T. I., Rybin V. G., Soldatkina O. A. New Tetracyclic Spiro-1,2,4-trioxolanes (Ozonides). Synthesis and Mass Spectrometric Study // Russian Journal of Organic Chemistry. 2019. Vol. 55. No. 1. pp. 101-107.
GOST all authors (up to 50) Copy
Akimova T. I., Rybin V. G., Soldatkina O. A. New Tetracyclic Spiro-1,2,4-trioxolanes (Ozonides). Synthesis and Mass Spectrometric Study // Russian Journal of Organic Chemistry. 2019. Vol. 55. No. 1. pp. 101-107.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1134/s1070428019010123
UR - https://doi.org/10.1134/s1070428019010123
TI - New Tetracyclic Spiro-1,2,4-trioxolanes (Ozonides). Synthesis and Mass Spectrometric Study
T2 - Russian Journal of Organic Chemistry
AU - Akimova, T I
AU - Rybin, V G
AU - Soldatkina, O A
PY - 2019
DA - 2019/01/01
PB - Pleiades Publishing
SP - 101-107
IS - 1
VL - 55
SN - 1070-4280
SN - 1608-3393
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2019_Akimova,
author = {T I Akimova and V G Rybin and O A Soldatkina},
title = {New Tetracyclic Spiro-1,2,4-trioxolanes (Ozonides). Synthesis and Mass Spectrometric Study},
journal = {Russian Journal of Organic Chemistry},
year = {2019},
volume = {55},
publisher = {Pleiades Publishing},
month = {jan},
url = {https://doi.org/10.1134/s1070428019010123},
number = {1},
pages = {101--107},
doi = {10.1134/s1070428019010123}
}
MLA
Cite this
MLA Copy
Akimova, T. I., et al. “New Tetracyclic Spiro-1,2,4-trioxolanes (Ozonides). Synthesis and Mass Spectrometric Study.” Russian Journal of Organic Chemistry, vol. 55, no. 1, Jan. 2019, pp. 101-107. https://doi.org/10.1134/s1070428019010123.