volume 58 issue 9 pages 1362-1367

Synthesis of Enantiomerically Pure Thioureas and Thiohydantoins Based on (R)- and (S)-1-(2,4-Dimethoxy-phenyl)ethan-1-amines

A A Barashkin 1
V S Polyakov 1
N L Shikut 1
A D Putilova 1
A R Gorovoy 1
V. A. Tafeenko 1
N. V. Zyk 1
Publication typeJournal Article
Publication date2022-09-01
scimago Q4
wos Q4
SJR0.190
CiteScore1.3
Impact factor0.9
ISSN10704280, 16083393
Organic Chemistry
Abstract
A convenient procedure has been proposed for the isolation of R and S enantiomers of 1-(2,4-di­methoxyphenyl)ethan-1-amine from the racemate using di-O-benzoyltartaric acids as chiral auxiliaries. The pure enantiomers were converted into the corresponding chiral thioureas and 2-thiohydantoins by reaction with ethyl 2-isothiocyanatoacetate.
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GOST Copy
Barashkin A. A. et al. Synthesis of Enantiomerically Pure Thioureas and Thiohydantoins Based on (R)- and (S)-1-(2,4-Dimethoxy-phenyl)ethan-1-amines // Russian Journal of Organic Chemistry. 2022. Vol. 58. No. 9. pp. 1362-1367.
GOST all authors (up to 50) Copy
Barashkin A. A., Polyakov V. S., Shikut N. L., Putilova A. D., Gorovoy A. R., Tafeenko V. A., Zyk N. V., Beloglazkina E. K. Synthesis of Enantiomerically Pure Thioureas and Thiohydantoins Based on (R)- and (S)-1-(2,4-Dimethoxy-phenyl)ethan-1-amines // Russian Journal of Organic Chemistry. 2022. Vol. 58. No. 9. pp. 1362-1367.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1134/s1070428022090251
UR - https://link.springer.com/10.1134/S1070428022090251
TI - Synthesis of Enantiomerically Pure Thioureas and Thiohydantoins Based on (R)- and (S)-1-(2,4-Dimethoxy-phenyl)ethan-1-amines
T2 - Russian Journal of Organic Chemistry
AU - Barashkin, A A
AU - Polyakov, V S
AU - Shikut, N L
AU - Putilova, A D
AU - Gorovoy, A R
AU - Tafeenko, V. A.
AU - Zyk, N. V.
AU - Beloglazkina, E K
PY - 2022
DA - 2022/09/01
PB - Pleiades Publishing
SP - 1362-1367
IS - 9
VL - 58
SN - 1070-4280
SN - 1608-3393
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2022_Barashkin,
author = {A A Barashkin and V S Polyakov and N L Shikut and A D Putilova and A R Gorovoy and V. A. Tafeenko and N. V. Zyk and E K Beloglazkina},
title = {Synthesis of Enantiomerically Pure Thioureas and Thiohydantoins Based on (R)- and (S)-1-(2,4-Dimethoxy-phenyl)ethan-1-amines},
journal = {Russian Journal of Organic Chemistry},
year = {2022},
volume = {58},
publisher = {Pleiades Publishing},
month = {sep},
url = {https://link.springer.com/10.1134/S1070428022090251},
number = {9},
pages = {1362--1367},
doi = {10.1134/s1070428022090251}
}
MLA
Cite this
MLA Copy
Barashkin, A. A., et al. “Synthesis of Enantiomerically Pure Thioureas and Thiohydantoins Based on (R)- and (S)-1-(2,4-Dimethoxy-phenyl)ethan-1-amines.” Russian Journal of Organic Chemistry, vol. 58, no. 9, Sep. 2022, pp. 1362-1367. https://link.springer.com/10.1134/S1070428022090251.