THE PREPARATION OF SOME THIOSEMICARBAZONES AND THEIR COPPER COMPLEXES: PART III
Тип публикации: Journal Article
Дата публикации: 1962-06-01
scimago Q3
wos Q4
БС3
SJR: 0.254
CiteScore: 2
Impact factor: 1
ISSN: 00084042, 14803291
General Chemistry
Catalysis
Organic Chemistry
Краткое описание
Reactions of some diketones with thiosemicarbazide have been studied under various conditions. Monothiosemicarbazones, dithiosemicarbazones, and cyclization products can be obtained. It was found that dithiosemicarbazones form 1:1 complexes with Cu(II) but failed to react with Cu(I). Dithiosemicarbazones in which the N2-hydrogen atom has been replaced by Me do not form complexes, confirming our views about the importance of this hydrogen atom in the thione ↔ thiol tautomerism necessary for complex formation. 4,4-Dimethyldithiosemicarbazones behave like the unsubstituted parent compounds in forming 1:1 complexes with Cu(II). Infrared spectra provide evidence for the structure of a cyclization product, 5,6-diphenyl-3-thio-1,2,4-triazine, which had been erroneously described by various authors as the thiol tautomer, 5,6-diphenyl-3-mercapto-1,2,4-triazine.
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108
Всего цитирований:
108
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MLA
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ГОСТ
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Gingras B. A., Suprunchuk T., Bayley C. H. THE PREPARATION OF SOME THIOSEMICARBAZONES AND THEIR COPPER COMPLEXES: PART III // Canadian Journal of Chemistry. 1962. Vol. 40. No. 6. pp. 1053-1059.
ГОСТ со всеми авторами (до 50)
Скопировать
Gingras B. A., Suprunchuk T., Bayley C. H. THE PREPARATION OF SOME THIOSEMICARBAZONES AND THEIR COPPER COMPLEXES: PART III // Canadian Journal of Chemistry. 1962. Vol. 40. No. 6. pp. 1053-1059.
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RIS
Скопировать
TY - JOUR
DO - 10.1139/v62-161
UR - https://doi.org/10.1139/v62-161
TI - THE PREPARATION OF SOME THIOSEMICARBAZONES AND THEIR COPPER COMPLEXES: PART III
T2 - Canadian Journal of Chemistry
AU - Gingras, B. A.
AU - Suprunchuk, T.
AU - Bayley, C. H.
PY - 1962
DA - 1962/06/01
PB - Canadian Science Publishing
SP - 1053-1059
IS - 6
VL - 40
SN - 0008-4042
SN - 1480-3291
ER -
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BibTex (до 50 авторов)
Скопировать
@article{1962_Gingras,
author = {B. A. Gingras and T. Suprunchuk and C. H. Bayley},
title = {THE PREPARATION OF SOME THIOSEMICARBAZONES AND THEIR COPPER COMPLEXES: PART III},
journal = {Canadian Journal of Chemistry},
year = {1962},
volume = {40},
publisher = {Canadian Science Publishing},
month = {jun},
url = {https://doi.org/10.1139/v62-161},
number = {6},
pages = {1053--1059},
doi = {10.1139/v62-161}
}
Цитировать
MLA
Скопировать
Gingras, B. A., et al. “THE PREPARATION OF SOME THIOSEMICARBAZONES AND THEIR COPPER COMPLEXES: PART III.” Canadian Journal of Chemistry, vol. 40, no. 6, Jun. 1962, pp. 1053-1059. https://doi.org/10.1139/v62-161.