Molecular Structure of Nitro- and Nitrito-Copper Complexes as Reaction Intermediates in Electrochemical Reduction of Nitrite to Dinitrogen Oxide
Тип публикации: Journal Article
Дата публикации: 1995-03-01
scimago Q2
wos Q2
БС1
SJR: 0.678
CiteScore: 7
Impact factor: 3.8
ISSN: 00092673, 13480634
General Chemistry
Краткое описание
Copper-nitrito and -nitro isomers, [Cu(ONO)(tpa)]PF6 and [Cu(NO2)(tpa)]PF6 (tpa = tris[(2-pyridyl)methyl]amine) were isolated and the molecular structures were determined by X-ray analysis. [Cu(ONO)(tpa)]PF6 (C18H18N5O2PF6Cu) crystallizes in the monoclinic space group P21/a with a = 13.374(2), b = 14.033(2), c = 13.455(2) A, β = 119.10(1)°, V = 2206.5(6) A3, and Z = 4. [Cu(NO2)(tpa)]PF6 (C18H18N5O2PF6Cu) crystallizes in the orthorhombic space group I/ba2 with a = 16.718(3), b = 17.554(3), c = 14.785(3) A, V = 4338(1) A3, and Z = 8. Those nitrito- and nitro-complexes exist as an equilibrium mixture in solutions. Electrochemical reduction of NO2− in the presence of [Cu(H2O)(tpa)](ClO4)2 at −0.4 V in H2O (pH 7.0) catalytically produced N2O with concomitant evolution of a small amount of NO via the nitro and nitrito adducts.
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Komeda N. et al. Molecular Structure of Nitro- and Nitrito-Copper Complexes as Reaction Intermediates in Electrochemical Reduction of Nitrite to Dinitrogen Oxide // Bulletin of the Chemical Society of Japan. 1995. Vol. 68. No. 2. pp. 581-589.
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Komeda N., NAGAO H., Kushi Y., Adachi G., Suzuki M., UEHARA A., Tanaka K. Molecular Structure of Nitro- and Nitrito-Copper Complexes as Reaction Intermediates in Electrochemical Reduction of Nitrite to Dinitrogen Oxide // Bulletin of the Chemical Society of Japan. 1995. Vol. 68. No. 2. pp. 581-589.
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TY - JOUR
DO - 10.1246/bcsj.68.581
UR - https://doi.org/10.1246/bcsj.68.581
TI - Molecular Structure of Nitro- and Nitrito-Copper Complexes as Reaction Intermediates in Electrochemical Reduction of Nitrite to Dinitrogen Oxide
T2 - Bulletin of the Chemical Society of Japan
AU - Komeda, Nobutoshi
AU - NAGAO, Hirotaka
AU - Kushi, Yoshinori
AU - Adachi, Gin‐ya
AU - Suzuki, Masatatsu
AU - UEHARA, Akira
AU - Tanaka, Koji
PY - 1995
DA - 1995/03/01
PB - Oxford University Press
SP - 581-589
IS - 2
VL - 68
SN - 0009-2673
SN - 1348-0634
ER -
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@article{1995_Komeda,
author = {Nobutoshi Komeda and Hirotaka NAGAO and Yoshinori Kushi and Gin‐ya Adachi and Masatatsu Suzuki and Akira UEHARA and Koji Tanaka},
title = {Molecular Structure of Nitro- and Nitrito-Copper Complexes as Reaction Intermediates in Electrochemical Reduction of Nitrite to Dinitrogen Oxide},
journal = {Bulletin of the Chemical Society of Japan},
year = {1995},
volume = {68},
publisher = {Oxford University Press},
month = {mar},
url = {https://doi.org/10.1246/bcsj.68.581},
number = {2},
pages = {581--589},
doi = {10.1246/bcsj.68.581}
}
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MLA
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Komeda, Nobutoshi, et al. “Molecular Structure of Nitro- and Nitrito-Copper Complexes as Reaction Intermediates in Electrochemical Reduction of Nitrite to Dinitrogen Oxide.” Bulletin of the Chemical Society of Japan, vol. 68, no. 2, Mar. 1995, pp. 581-589. https://doi.org/10.1246/bcsj.68.581.