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8,18-dithia-1,4,11,14-tetraazapentacyclo[11.7.0.03,11.05,9. 015,19]icosa-3,5(9),6,13,15(19),16-hexaene-10,20-dione
Oleg A. Rakitin
1, 2
Publication type: Journal Article
Publication date: 2019-04-13
DOI:
10.3390/M1056
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
4H-3λ2-Thieno[3,2-d]pyrimidin-4-one derivatives are of interest as biologically active compounds. In this communication, 2-(chloromethyl)-4H-3λ2-thieno[3,2-d]pyrimidin-4-one (1) was investigated in the reaction with ammonia, potassium phthalimide, and other basic agents. The dimerization product—8,18-dithia-1,4,11,14-tetrazapentacyclo[11.7.0.03,11.05,9.015,19]icosa-3,5(9),6,13,15(19),16-hexaene-10,20-dione was formed in the reaction with potassium phthalimide in DMF, by heating at 110 °C for 5 h. The structure of the newly synthesized compound was established by means of elemental analysis, high resolution mass-spectrometry, 1H, 13C NMR, and IR spectroscopy, and mass-spectrometry.
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Ogurtsov V. A., Rakitin O. A. 8,18-dithia-1,4,11,14-tetraazapentacyclo[11.7.0.03,11.05,9. 015,19]icosa-3,5(9),6,13,15(19),16-hexaene-10,20-dione // MolBank. 2019. Vol. 2019. No. 2. p. M1056.
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Ogurtsov V. A., Rakitin O. A. 8,18-dithia-1,4,11,14-tetraazapentacyclo[11.7.0.03,11.05,9. 015,19]icosa-3,5(9),6,13,15(19),16-hexaene-10,20-dione // MolBank. 2019. Vol. 2019. No. 2. p. M1056.
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TY - JOUR
DO - 10.3390/M1056
UR - https://www.mdpi.com/1422-8599/2019/2/M1056
TI - 8,18-dithia-1,4,11,14-tetraazapentacyclo[11.7.0.03,11.05,9. 015,19]icosa-3,5(9),6,13,15(19),16-hexaene-10,20-dione
T2 - MolBank
AU - Ogurtsov, Vladimir A.
AU - Rakitin, Oleg A.
PY - 2019
DA - 2019/04/13
PB - MDPI
SP - M1056
IS - 2
VL - 2019
SN - 1422-8599
ER -
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@article{2019_Ogurtsov,
author = {Vladimir A. Ogurtsov and Oleg A. Rakitin},
title = {8,18-dithia-1,4,11,14-tetraazapentacyclo[11.7.0.03,11.05,9. 015,19]icosa-3,5(9),6,13,15(19),16-hexaene-10,20-dione},
journal = {MolBank},
year = {2019},
volume = {2019},
publisher = {MDPI},
month = {apr},
url = {https://www.mdpi.com/1422-8599/2019/2/M1056},
number = {2},
pages = {M1056},
doi = {10.3390/M1056}
}
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Ogurtsov, Vladimir A., et al. “8,18-dithia-1,4,11,14-tetraazapentacyclo[11.7.0.03,11.05,9. 015,19]icosa-3,5(9),6,13,15(19),16-hexaene-10,20-dione.” MolBank, vol. 2019, no. 2, Apr. 2019, p. M1056. https://www.mdpi.com/1422-8599/2019/2/M1056.