Open Access
Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate
Timofey N Chmovzh
1, 2
,
Oleg A. Rakitin
1, 2
Publication type: Journal Article
Publication date: 2021-07-05
DOI:
10.3390/M1247
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
New donor building blocks, i.e., triarylamino derivatives, are of great interest for the production of organic photovoltaic materials. In this communication, bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)amine was synthesized in a two-step process via hydrolysis of its tert-butyl carbamate derivative. tert-Butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate was obtained by Suzuki cross-coupling reaction of tert-butyl bis(4-bromophenyl)carbamate and (4-(hexyloxy)phenyl)boronic acid in the presence of tetrakis(triphenylphosphine)palladium(0). The structure of newly synthesized compounds was established by means of elemental analysis, high resolution mass-spectrometry, 1H, 13C-NMR, IR and UV spectroscopy and mass-spectrometry.
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Chmovzh T. N. et al. Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate // MolBank. 2021. Vol. 2021. No. 3. p. M1247.
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Chmovzh T. N., Rakitin O. A. Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate // MolBank. 2021. Vol. 2021. No. 3. p. M1247.
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TY - JOUR
DO - 10.3390/M1247
UR - https://www.mdpi.com/1422-8599/2021/3/M1247
TI - Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate
T2 - MolBank
AU - Chmovzh, Timofey N
AU - Rakitin, Oleg A.
PY - 2021
DA - 2021/07/05
PB - MDPI
SP - M1247
IS - 3
VL - 2021
SN - 1422-8599
ER -
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@article{2021_Chmovzh,
author = {Timofey N Chmovzh and Oleg A. Rakitin},
title = {Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate},
journal = {MolBank},
year = {2021},
volume = {2021},
publisher = {MDPI},
month = {jul},
url = {https://www.mdpi.com/1422-8599/2021/3/M1247},
number = {3},
pages = {M1247},
doi = {10.3390/M1247}
}
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MLA
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Chmovzh, Timofey N., et al. “Tert-butyl bis(4′-(hexyloxy)-[1,1′-biphenyl]-4-yl)carbamate.” MolBank, vol. 2021, no. 3, Jul. 2021, p. M1247. https://www.mdpi.com/1422-8599/2021/3/M1247.
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