Open Access
4,7-bis(Dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine
Publication type: Journal Article
Publication date: 2021-10-25
DOI:
10.3390/M1291
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
Bis(alkylsulfanyl) derivatives of 1,2,5-thiadiazoles fused with aromatic and heteroaromatic rings containing long alkyl chains are of interest as compounds with liquid crystalline properties. In this communication, 4,7-bis(dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine 1 was obtained from 4,7-dibromo-[1,2,5]thiadiazolo[3,4-c]pyridine 2 by a combination of two reactions—aromatic nucleophilic substitution SNAr and Buchwald–Hartwig cross-coupling. The structure of the newly synthesized compounds was established by means of elemental analysis; high-resolution mass spectrometry; 1H, 13C NMR, IR and UV spectroscopy; and mass spectrometry.
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Chmovzh T. N. et al. 4,7-bis(Dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine // MolBank. 2021. Vol. 2021. No. 4. p. M1291.
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Chmovzh T. N., Kudryashev T. A., Rakitin O. A. 4,7-bis(Dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine // MolBank. 2021. Vol. 2021. No. 4. p. M1291.
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TY - JOUR
DO - 10.3390/M1291
UR - https://www.mdpi.com/1422-8599/2021/4/M1291
TI - 4,7-bis(Dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine
T2 - MolBank
AU - Chmovzh, Timofey N
AU - Kudryashev, Timofey A
AU - Rakitin, Oleg A.
PY - 2021
DA - 2021/10/25
PB - MDPI
SP - M1291
IS - 4
VL - 2021
SN - 1422-8599
ER -
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@article{2021_Chmovzh,
author = {Timofey N Chmovzh and Timofey A Kudryashev and Oleg A. Rakitin},
title = {4,7-bis(Dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine},
journal = {MolBank},
year = {2021},
volume = {2021},
publisher = {MDPI},
month = {oct},
url = {https://www.mdpi.com/1422-8599/2021/4/M1291},
number = {4},
pages = {M1291},
doi = {10.3390/M1291}
}
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MLA
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Chmovzh, Timofey N., et al. “4,7-bis(Dodecylthio)-[1,2,5]thiadiazolo[3,4-c]pyridine.” MolBank, vol. 2021, no. 4, Oct. 2021, p. M1291. https://www.mdpi.com/1422-8599/2021/4/M1291.