Open Access
MolBank, volume 2022, issue 2, pages M1371
5,5’‐Thiobis(4‐chloro‐3H‐1,2‐dithiole‐3‐thione)
Publication type: Journal Article
Publication date: 2022-05-27
DOI:
10.3390/M1371
Organic Chemistry
Biochemistry
Physical and Theoretical Chemistry
Abstract
3H-1,2-Dithiole-3-thiones are important compounds with many types of significant pharmacological activity. Although many derivatives of this class have been described in the literature, their thioethers have not previously been obtained. In this communication, it is shown that the reaction of 4,5-dichloro-3H-1,2-dithiole-3-thione with potassium isocyanate unexpectedly gave 5,5′-thiobis(4-chloro-3H-1,2-dithiole-3-thione). The structure of the synthesized compound was established by elemental analysis, high-resolution mass spectrometry, 13C NMR and IR spectroscopy, and mass spectrometry.
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Progress in Heterocyclic Chemistry
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Progress in Heterocyclic Chemistry
1 publication, 100%
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Elsevier
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Elsevier
1 publication, 100%
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Ogurtsov V. A., Rakitin O. A. 5,5’‐Thiobis(4‐chloro‐3H‐1,2‐dithiole‐3‐thione) // MolBank. 2022. Vol. 2022. No. 2. p. M1371.
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Ogurtsov V. A., Rakitin O. A. 5,5’‐Thiobis(4‐chloro‐3H‐1,2‐dithiole‐3‐thione) // MolBank. 2022. Vol. 2022. No. 2. p. M1371.
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TY - JOUR
DO - 10.3390/M1371
UR - https://doi.org/10.3390%2FM1371
TI - 5,5’‐Thiobis(4‐chloro‐3H‐1,2‐dithiole‐3‐thione)
T2 - MolBank
AU - Ogurtsov, Vladimir A.
AU - Rakitin, Oleg A.
PY - 2022
DA - 2022/05/27 00:00:00
PB - Multidisciplinary Digital Publishing Institute (MDPI)
SP - M1371
IS - 2
VL - 2022
SN - 1422-8599
ER -
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@article{2022_Ogurtsov,
author = {Vladimir A. Ogurtsov and Oleg A. Rakitin},
title = {5,5’‐Thiobis(4‐chloro‐3H‐1,2‐dithiole‐3‐thione)},
journal = {MolBank},
year = {2022},
volume = {2022},
publisher = {Multidisciplinary Digital Publishing Institute (MDPI)},
month = {may},
url = {https://doi.org/10.3390%2FM1371},
number = {2},
pages = {M1371},
doi = {10.3390/M1371}
}
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Ogurtsov, Vladimir A., and Oleg A. Rakitin. “5,5’‐Thiobis(4‐chloro‐3H‐1,2‐dithiole‐3‐thione).” MolBank, vol. 2022, no. 2, May. 2022, p. M1371. https://doi.org/10.3390%2FM1371.