Molecular Structure of 1,2,5-Selenadiazolodibenzosubporphyrazinatoboron(III) Chloride and Influence of Perfluorination and Perchlorination on Its Spectral Properties
Publication type: Journal Article
Publication date: 2020-05-19
scimago Q4
wos Q3
SJR: 0.193
CiteScore: 1.5
Impact factor: 1.2
ISSN: 19989539, 27131092
Organic Chemistry
Analytical Chemistry
Abstract
Novel Se-containing heterocyclic subphthalocyanine analogue – (1,2,5-selenadiazolo)dibenzosubporphyrazinatoboron(III) chloride 3a was prepared by template cross-cyclomerization of 1,2,5-selenadiazolo-3,4-dicarbonitrile 1 and phthalonitrile 2a with BCl3 in p-xylene. Similar reactions of 1 and tetrafluoroor tetrachlorphthalonitriles (2b or 2c) afford octafluorinated and octachlorinated subporphyrazines 3b and 3c. The formation of 3a-c was established by MALDI-TOF mass-spectrometry and the structure of 3a was determined by single crystal X-ray diffraction. Influence of halogenation on the spectral properties is discussed.
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Hamdoush M. et al. Molecular Structure of 1,2,5-Selenadiazolodibenzosubporphyrazinatoboron(III) Chloride and Influence of Perfluorination and Perchlorination on Its Spectral Properties // Macroheterocycles. 2020. Vol. 13. No. 1. pp. 19-22.
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Hamdoush M., Somov N. V., Ivanova S. S., Stuzhin P. A. Molecular Structure of 1,2,5-Selenadiazolodibenzosubporphyrazinatoboron(III) Chloride and Influence of Perfluorination and Perchlorination on Its Spectral Properties // Macroheterocycles. 2020. Vol. 13. No. 1. pp. 19-22.
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TY - JOUR
DO - 10.6060/mhc190970s
UR - https://macroheterocycles.isuct.ru/en/mhc190970s
TI - Molecular Structure of 1,2,5-Selenadiazolodibenzosubporphyrazinatoboron(III) Chloride and Influence of Perfluorination and Perchlorination on Its Spectral Properties
T2 - Macroheterocycles
AU - Hamdoush, Mahmoud
AU - Somov, Nikolay V.
AU - Ivanova, Svetlana S.
AU - Stuzhin, Pavel A.
PY - 2020
DA - 2020/05/19
PB - Ivanovo State University of Chemistry and Technology
SP - 19-22
IS - 1
VL - 13
SN - 1998-9539
SN - 2713-1092
ER -
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@article{2020_Hamdoush,
author = {Mahmoud Hamdoush and Nikolay V. Somov and Svetlana S. Ivanova and Pavel A. Stuzhin},
title = {Molecular Structure of 1,2,5-Selenadiazolodibenzosubporphyrazinatoboron(III) Chloride and Influence of Perfluorination and Perchlorination on Its Spectral Properties},
journal = {Macroheterocycles},
year = {2020},
volume = {13},
publisher = {Ivanovo State University of Chemistry and Technology},
month = {may},
url = {https://macroheterocycles.isuct.ru/en/mhc190970s},
number = {1},
pages = {19--22},
doi = {10.6060/mhc190970s}
}
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Hamdoush, Mahmoud, et al. “Molecular Structure of 1,2,5-Selenadiazolodibenzosubporphyrazinatoboron(III) Chloride and Influence of Perfluorination and Perchlorination on Its Spectral Properties.” Macroheterocycles, vol. 13, no. 1, May. 2020, pp. 19-22. https://macroheterocycles.isuct.ru/en/mhc190970s.
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