Chemical Engineering Journal, volume 430, pages 132670
Development of 3D+G printing for the design of customizable flow reactors
Publication type: Journal Article
Publication date: 2022-02-01
Journal:
Chemical Engineering Journal
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor: 15.1
ISSN: 13858947
General Chemistry
General Chemical Engineering
Industrial and Manufacturing Engineering
Environmental Chemistry
Abstract
A novel approach to creating flow reactors was developed that combines 3D printing of the reactor core by fused deposition modeling using conventional plastic materials, followed by chemical/galvanic plating of the resulting piece («3D+G printing»). Complete reactor assembly was successfully tested in a variety of chemical processes. Designed flow reactors are characterized by chemical resistance, versatile geometry, modular design, and excellent operating performance. • Developed 3D+G printing process enables fabrication of the solvent-resistant flow reactors of a custom shape. • Complete 3D+G printed flow reactor assembly was formulated and tested in various chemical processes. • Innovative combination of 3D printing with galvanic metal plating increases the resistance of the printed part. • SEM study reveals complete metal coverage of all micro-imperfections of the plastic core. An in-depth study of chemical processes at plastic-metal interfaces led to the development of a novel approach to the creation of lab-on-a-chip microflow reactors. The developed method combines 3D printing of the reactor core by fused deposition modeling using conventional plastic material (ABS), followed by chemical (electroless copper) and galvanic plating (nickel) of the resulting piece (in overall, 3D+G printing process). Detailed analysis of the pieces along all 3D+G stages by electron microscopy revealed step-by-step processes on the plastic-metal interface, which finally allowed innovative reactor design. Despite being made from low-cost materials in a simple procedure, flow reactors are characterized by chemical resistance, versatile geometry, modular design and excellent operating performance. Complete reactor assembly was formulated and successfully tested in a variety of chemical processes targeted on biologically active molecules, including homogeneous, heterogeneous and photochemical reactions. Reactor modules can be combined into cascades to perform sequential reactions. Metallized reactors can be used multiple times in a variety of chemical processes.
Citations by journals
|
1
|
|
|
Micromachines
|
Micromachines
1 publication, 6.25%
|
|
Materials
|
Materials
1 publication, 6.25%
|
|
Processes
|
Processes
1 publication, 6.25%
|
|
Scientific Reports
|
Scientific Reports
1 publication, 6.25%
|
|
Chemical Engineering and Processing: Process Intensification
|
Chemical Engineering and Processing: Process Intensification
1 publication, 6.25%
|
|
Reaction Chemistry and Engineering
|
Reaction Chemistry and Engineering
1 publication, 6.25%
|
|
Applied Materials Today
|
Applied Materials Today
1 publication, 6.25%
|
|
ACS Sustainable Chemistry and Engineering
|
ACS Sustainable Chemistry and Engineering
1 publication, 6.25%
|
|
Chemical Engineering Journal
|
Chemical Engineering Journal
1 publication, 6.25%
|
|
Materials and Design
|
Materials and Design
1 publication, 6.25%
|
|
Organic Process Research and Development
|
Organic Process Research and Development
1 publication, 6.25%
|
|
Inventions
|
Inventions
1 publication, 6.25%
|
|
JACS Au
|
JACS Au
1 publication, 6.25%
|
|
Green Chemistry
|
Green Chemistry
1 publication, 6.25%
|
|
1
|
Citations by publishers
|
1
2
3
4
|
|
|
Multidisciplinary Digital Publishing Institute (MDPI)
|
Multidisciplinary Digital Publishing Institute (MDPI)
4 publications, 25%
|
|
Elsevier
|
Elsevier
4 publications, 25%
|
|
Royal Society of Chemistry (RSC)
|
Royal Society of Chemistry (RSC)
3 publications, 18.75%
|
|
American Chemical Society (ACS)
|
American Chemical Society (ACS)
3 publications, 18.75%
|
|
Springer Nature
|
Springer Nature
1 publication, 6.25%
|
|
1
2
3
4
|
- We do not take into account publications that without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
{"yearsCitations":{"type":"bar","data":{"show":true,"labels":[2022,2023,2024],"ids":[0,0,0],"codes":[0,0,0],"imageUrls":["","",""],"datasets":[{"label":"Citations number","data":[5,9,2],"backgroundColor":["#3B82F6","#3B82F6","#3B82F6"],"percentage":["31.25","56.25","12.5"],"barThickness":null}]},"options":{"indexAxis":"x","maintainAspectRatio":true,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"}},"x":{"ticks":{"stepSize":1,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"}}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Citations per year","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}},"journals":{"type":"bar","data":{"show":true,"labels":["Micromachines","Materials","Processes","Scientific Reports","Chemical Engineering and Processing: Process Intensification","Reaction Chemistry and Engineering","Applied Materials Today","ACS Sustainable Chemistry and Engineering","Chemical Engineering Journal","Materials and Design","Organic Process Research and Development","Inventions","JACS Au","Green Chemistry"],"ids":[1083,25198,19796,13767,12038,20057,7900,18886,16275,8941,11058,11012,26622,1017],"codes":[0,0,0,0,0,0,0,0,0,0,0,0,0,0],"imageUrls":["\/storage\/images\/resized\/MjH1ITP7lMYGxeqUZfkt2BnVLgjkk413jwBV97XX_medium.webp","\/storage\/images\/resized\/MjH1ITP7lMYGxeqUZfkt2BnVLgjkk413jwBV97XX_medium.webp","\/storage\/images\/resized\/MjH1ITP7lMYGxeqUZfkt2BnVLgjkk413jwBV97XX_medium.webp","\/storage\/images\/resized\/voXLqlsvTwv5p3iMQ8Dhs95nqB4AXOG7Taj7G4ra_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/leiAYcRDGTSl5B1eCnwpSGqmDEUEfDPPoYisFGhT_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/MjH1ITP7lMYGxeqUZfkt2BnVLgjkk413jwBV97XX_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/leiAYcRDGTSl5B1eCnwpSGqmDEUEfDPPoYisFGhT_medium.webp"],"datasets":[{"label":"","data":[1,1,1,1,1,1,1,1,1,1,1,1,1,1],"backgroundColor":["#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6"],"percentage":[6.25,6.25,6.25,6.25,6.25,6.25,6.25,6.25,6.25,6.25,6.25,6.25,6.25,6.25],"barThickness":13}]},"options":{"indexAxis":"y","maintainAspectRatio":false,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"}},"x":{"ticks":{"stepSize":null,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"}}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Journals","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}},"publishers":{"type":"bar","data":{"show":true,"labels":["Multidisciplinary Digital Publishing Institute (MDPI)","Elsevier","Royal Society of Chemistry (RSC)","American Chemical Society (ACS)","Springer Nature"],"ids":[202,17,123,40,8],"codes":[0,0,0,0,0],"imageUrls":["\/storage\/images\/resized\/MjH1ITP7lMYGxeqUZfkt2BnVLgjkk413jwBV97XX_medium.webp","\/storage\/images\/resized\/GDnYOu1UpMMfMMRV6Aqle4H0YLLsraeD9IP9qScG_medium.webp","\/storage\/images\/resized\/leiAYcRDGTSl5B1eCnwpSGqmDEUEfDPPoYisFGhT_medium.webp","\/storage\/images\/resized\/iLiQsFqFaSEx6chlGQ5fbAwF6VYU3WWa08hkss0g_medium.webp","\/storage\/images\/resized\/voXLqlsvTwv5p3iMQ8Dhs95nqB4AXOG7Taj7G4ra_medium.webp"],"datasets":[{"label":"","data":[4,4,3,3,1],"backgroundColor":["#3B82F6","#3B82F6","#3B82F6","#3B82F6","#3B82F6"],"percentage":[25,25,18.75,18.75,6.25],"barThickness":13}]},"options":{"indexAxis":"y","maintainAspectRatio":false,"scales":{"y":{"ticks":{"precision":0,"autoSkip":false,"font":{"family":"Montserrat"},"color":"#000000"}},"x":{"ticks":{"stepSize":null,"precision":0,"font":{"family":"Montserrat"},"color":"#000000"}}},"plugins":{"legend":{"position":"top","labels":{"font":{"family":"Montserrat"},"color":"#000000"}},"title":{"display":true,"text":"Publishers","font":{"size":24,"family":"Montserrat","weight":600},"color":"#000000"}}}}}
Metrics
Cite this
GOST |
RIS |
BibTex
Cite this
GOST
Copy
Kucherov F. A. et al. Development of 3D+G printing for the design of customizable flow reactors // Chemical Engineering Journal. 2022. Vol. 430. p. 132670.
GOST all authors (up to 50)
Copy
Kucherov F. A., Romashov L. V., Ananikov V. P. Development of 3D+G printing for the design of customizable flow reactors // Chemical Engineering Journal. 2022. Vol. 430. p. 132670.
Cite this
RIS
Copy
TY - JOUR
DO - 10.1016/j.cej.2021.132670
UR - https://doi.org/10.1016%2Fj.cej.2021.132670
TI - Development of 3D+G printing for the design of customizable flow reactors
T2 - Chemical Engineering Journal
AU - Kucherov, Fedor A
AU - Romashov, Leonid V.
AU - Ananikov, Valentine P.
PY - 2022
DA - 2022/02/01 00:00:00
PB - Elsevier
SP - 132670
VL - 430
SN - 1385-8947
ER -
Cite this
BibTex
Copy
@article{2022_Kucherov,
author = {Fedor A Kucherov and Leonid V. Romashov and Valentine P. Ananikov},
title = {Development of 3D+G printing for the design of customizable flow reactors},
journal = {Chemical Engineering Journal},
year = {2022},
volume = {430},
publisher = {Elsevier},
month = {feb},
url = {https://doi.org/10.1016%2Fj.cej.2021.132670},
pages = {132670},
doi = {10.1016/j.cej.2021.132670}
}
Profiles