Heptanuclear Cage Cu II ‐Silsesquioxanes: Synthesis, Structure and Catalytic Activity
Тип публикации: Journal Article
Дата публикации: 2018-04-14
scimago Q2
wos Q3
БС2
SJR: 0.459
CiteScore: 3.9
Impact factor: 2.0
ISSN: 14341948, 10990682
Inorganic Chemistry
Краткое описание
Two prismatic phenyl‐ (PhSiO1.5)14(CuO)7 (1, 29 % yield) and methyl‐ (MeSiO1.5)14(CuO)7 (2, 19 % yield) heptacoppersilsesquioxanes were obtained by the interaction of Cu,Na‐based cage silsesquioxanes [(RSiO1.5)12(CuO)4(NaO0.5)4] (R = Ph, Me) with 4,4′‐bipyridine and pyrazine, respectively, acting as “silent witness” ligands. Unusual molecular topologies of both compounds 1 and 2, which are the first representatives of cage silsesquioxanes with seven metal ions in their cores, were established by X‐ray diffraction studies. Complex 1 was found to be an active precatalyst in the oxidation of alkanes and 1‐phenylethanol to alkyl hydroperoxides and acetophenone, respectively. Alkanes were oxidized by hydrogen peroxide, and the alcohol was oxidized by tert‐butyl hydroperoxide.
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Bilyachenko A. N. et al. Heptanuclear Cage Cu II ‐Silsesquioxanes: Synthesis, Structure and Catalytic Activity // European Journal of Inorganic Chemistry. 2018. Vol. 2018. No. 22. pp. 2505-2511.
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Bilyachenko A. N., Levitsky M. M., Korlyukov A., Korlyukov A. A., Khrustalev V. N., Zubavichus Y. V., Shul'pin G. B., Shubina E. S., Vologzhanina A., Vologzhanina A. V., Shulpin G. B. Heptanuclear Cage Cu II ‐Silsesquioxanes: Synthesis, Structure and Catalytic Activity // European Journal of Inorganic Chemistry. 2018. Vol. 2018. No. 22. pp. 2505-2511.
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TY - JOUR
DO - 10.1002/ejic.201701340
UR - https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201701340
TI - Heptanuclear Cage Cu II ‐Silsesquioxanes: Synthesis, Structure and Catalytic Activity
T2 - European Journal of Inorganic Chemistry
AU - Bilyachenko, Alexey N
AU - Levitsky, Mikhail M
AU - Korlyukov, Alexander
AU - Korlyukov, Alexander A.
AU - Khrustalev, Victor N.
AU - Zubavichus, Yan V.
AU - Shul'pin, Georgiy B.
AU - Shubina, Elena S.
AU - Vologzhanina, A.
AU - Vologzhanina, Anna V.
AU - Shulpin, Georgiy B
PY - 2018
DA - 2018/04/14
PB - Wiley
SP - 2505-2511
IS - 22
VL - 2018
SN - 1434-1948
SN - 1099-0682
ER -
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@article{2018_Bilyachenko,
author = {Alexey N Bilyachenko and Mikhail M Levitsky and Alexander Korlyukov and Alexander A. Korlyukov and Victor N. Khrustalev and Yan V. Zubavichus and Georgiy B. Shul'pin and Elena S. Shubina and A. Vologzhanina and Anna V. Vologzhanina and Georgiy B Shulpin},
title = {Heptanuclear Cage Cu II ‐Silsesquioxanes: Synthesis, Structure and Catalytic Activity},
journal = {European Journal of Inorganic Chemistry},
year = {2018},
volume = {2018},
publisher = {Wiley},
month = {apr},
url = {https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201701340},
number = {22},
pages = {2505--2511},
doi = {10.1002/ejic.201701340}
}
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MLA
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Bilyachenko, Alexey N., et al. “Heptanuclear Cage Cu II ‐Silsesquioxanes: Synthesis, Structure and Catalytic Activity.” European Journal of Inorganic Chemistry, vol. 2018, no. 22, Apr. 2018, pp. 2505-2511. https://chemistry-europe.onlinelibrary.wiley.com/doi/10.1002/ejic.201701340.