Novel paste electrodes based on phosphonium salt room temperature ionic liquids for studying the redox properties of insoluble compounds
M N Khrizanforov
1
,
D M Arkhipova
1
,
R P Shekurov
1
,
T P Gerasimova
1
,
V V Ermolaev
1
,
D R Islamov
1
,
V A Miluykov
1
,
O. N. Kataeva
1
,
V V Khrizanforova
1
,
O G Sinyashin
1
,
Publication type: Journal Article
Publication date: 2015-05-30
scimago Q2
wos Q3
SJR: 0.552
CiteScore: 4.6
Impact factor: 2.6
ISSN: 14328488, 14330768
Electrochemistry
Condensed Matter Physics
General Materials Science
Electrical and Electronic Engineering
Abstract
A new carbon paste electrode is described, which contains the room temperature ionic liquid (RTIL) tri(tert-butyl)(dodecyl)phosphonium tetrafluoroborate as binder. The advantages of this electrode are a high conductivity, very wide electrochemical window (5.6 V from 2.7 to −2.9 V, one of the widest ever reported for RTILs), stability in time, and reproducibility. This RTIL-carbon paste electrode (CPE) allows determining the current-voltage characteristics of redox-active compounds. Thus, the newly synthesized insoluble compound poly-tris(μ2-1,1′-ferrocenediyl-phenylhydrophosphinato-phenylphosphinato)-iron(III) tetrahydrofuran solvate {μ2-[FeII(η5-C5H4–P(PhOO)(η5-C5H4–P(PhOOH))]3FeIII}·THF was studied, and a quasi-reversible three-electron oxidation could be observed at a potential more positive than that of ferrocene. A comparison of voltammograms on the paraffin-CPE and on the novel RTIL-CPE shows the advantages of the latter.
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Khrizanforov M. N. et al. Novel paste electrodes based on phosphonium salt room temperature ionic liquids for studying the redox properties of insoluble compounds // Journal of Solid State Electrochemistry. 2015. Vol. 19. No. 9. pp. 2883-2890.
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Khrizanforov M. N., Arkhipova D. M., Shekurov R. P., Gerasimova T. P., Ermolaev V. V., Islamov D. R., Miluykov V. A., Kataeva O. N., Khrizanforova V. V., Sinyashin O. G., Budnikova Y. H. Novel paste electrodes based on phosphonium salt room temperature ionic liquids for studying the redox properties of insoluble compounds // Journal of Solid State Electrochemistry. 2015. Vol. 19. No. 9. pp. 2883-2890.
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TY - JOUR
DO - 10.1007/s10008-015-2901-0
UR - https://doi.org/10.1007/s10008-015-2901-0
TI - Novel paste electrodes based on phosphonium salt room temperature ionic liquids for studying the redox properties of insoluble compounds
T2 - Journal of Solid State Electrochemistry
AU - Khrizanforov, M N
AU - Arkhipova, D M
AU - Shekurov, R P
AU - Gerasimova, T P
AU - Ermolaev, V V
AU - Islamov, D R
AU - Miluykov, V A
AU - Kataeva, O. N.
AU - Khrizanforova, V V
AU - Sinyashin, O G
AU - Budnikova, Y H
PY - 2015
DA - 2015/05/30
PB - Springer Nature
SP - 2883-2890
IS - 9
VL - 19
SN - 1432-8488
SN - 1433-0768
ER -
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BibTex (up to 50 authors)
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@article{2015_Khrizanforov,
author = {M N Khrizanforov and D M Arkhipova and R P Shekurov and T P Gerasimova and V V Ermolaev and D R Islamov and V A Miluykov and O. N. Kataeva and V V Khrizanforova and O G Sinyashin and Y H Budnikova},
title = {Novel paste electrodes based on phosphonium salt room temperature ionic liquids for studying the redox properties of insoluble compounds},
journal = {Journal of Solid State Electrochemistry},
year = {2015},
volume = {19},
publisher = {Springer Nature},
month = {may},
url = {https://doi.org/10.1007/s10008-015-2901-0},
number = {9},
pages = {2883--2890},
doi = {10.1007/s10008-015-2901-0}
}
Cite this
MLA
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Khrizanforov, M. N., et al. “Novel paste electrodes based on phosphonium salt room temperature ionic liquids for studying the redox properties of insoluble compounds.” Journal of Solid State Electrochemistry, vol. 19, no. 9, May. 2015, pp. 2883-2890. https://doi.org/10.1007/s10008-015-2901-0.