Springer Nature
Russian Chemical Bulletin
,  volume 58 ,  issue 6 ,  pages 1264-1269

4,5-Dihydroxyimidazolidin-2-ones in a-ureidoalkylation of N-carboxy-, N-hydroxy-, and N-aminoalkylureas 2. α-Ureidoalkylation of N-(hydroxyalkyl)ureas

Publication type: Journal Article
Publication date: 2009-06-01
Springer Nature
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The α-ureidoalkylation of N-(hydroxyalkyl)ureas (ureido alcohols) with 1,3-H2- and 1,3-Me2-4,5-dihydroxyimidazolidin-2-ones was systematically studied. The yields of glycolurils decrease both in going from 1,3-H2- to 1,3-Me2-4,5-dihydroxyimidazolidin-2-one and with increasing length (or with branching) of the hydroxyalkyl chain in ureido alcohols. The optimal reaction time for ureido alcohols is 1 h. The X-ray diffraction study showed that 2-(2-hydroxy-1,1-dimethylethyl)glycoluril crystallizes as a conglomerate. The enantiomeric analysis of 2-(2-hydroxyethyl)glycoluril was carried out by chiral-phase HPLC.
Found 
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Kravchenko A. N. et al. 4,5-Dihydroxyimidazolidin-2-ones in a-ureidoalkylation of N-carboxy-, N-hydroxy-, and N-aminoalkylureas 2. α-Ureidoalkylation of N-(hydroxyalkyl)ureas // Russian Chemical Bulletin. 2009. Vol. 58. No. 6. pp. 1264-1269.
GOST all authors (up to 50) Copy
Kravchenko A. N., Sigachev A. S., Belyakov P. A., Ilyin M. M., Lyssenko K., Davankov V. A., Lebedev O. V., Makhova N. N., Tartakovsky V. 4,5-Dihydroxyimidazolidin-2-ones in a-ureidoalkylation of N-carboxy-, N-hydroxy-, and N-aminoalkylureas 2. α-Ureidoalkylation of N-(hydroxyalkyl)ureas // Russian Chemical Bulletin. 2009. Vol. 58. No. 6. pp. 1264-1269.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1007/s11172-009-0165-5
UR - http://link.springer.com/10.1007/s11172-009-0165-5
TI - 4,5-Dihydroxyimidazolidin-2-ones in a-ureidoalkylation of N-carboxy-, N-hydroxy-, and N-aminoalkylureas 2. α-Ureidoalkylation of N-(hydroxyalkyl)ureas
T2 - Russian Chemical Bulletin
AU - Kravchenko, A N
AU - Sigachev, A S
AU - Belyakov, P A
AU - Ilyin, M. M.
AU - Lyssenko, K.A.
AU - Davankov, V. A.
AU - Lebedev, O V
AU - Makhova, N N
AU - Tartakovsky, V.A.
PY - 2009
DA - 2009/06/01
PB - Springer Nature
SP - 1264-1269
IS - 6
VL - 58
SN - 1066-5285
SN - 1573-9171
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2009_Kravchenko,
author = {A N Kravchenko and A S Sigachev and P A Belyakov and M. M. Ilyin and K.A. Lyssenko and V. A. Davankov and O V Lebedev and N N Makhova and V.A. Tartakovsky},
title = {4,5-Dihydroxyimidazolidin-2-ones in a-ureidoalkylation of N-carboxy-, N-hydroxy-, and N-aminoalkylureas 2. α-Ureidoalkylation of N-(hydroxyalkyl)ureas},
journal = {Russian Chemical Bulletin},
year = {2009},
volume = {58},
publisher = {Springer Nature},
month = {jun},
url = {http://link.springer.com/10.1007/s11172-009-0165-5},
number = {6},
pages = {1264--1269},
doi = {10.1007/s11172-009-0165-5}
}
MLA
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MLA Copy
Kravchenko, A. N., et al. “4,5-Dihydroxyimidazolidin-2-ones in a-ureidoalkylation of N-carboxy-, N-hydroxy-, and N-aminoalkylureas 2. α-Ureidoalkylation of N-(hydroxyalkyl)ureas.” Russian Chemical Bulletin, vol. 58, no. 6, Jun. 2009, pp. 1264-1269. http://link.springer.com/10.1007/s11172-009-0165-5.