4,5-dihydroxyimidazolidin-2-ones in an α-ureidoalkylation reaction of N-(carboxyalkyl)-, N-(hydroxyalkyl)-, and N-(aminoalkyl)ureas 3. * α-Ureidoalkylation of N-[2-(dimethylamino)ethyl]urea
G A Gazieva
1
,
P V Lozhkin
1
,
V.V. Baranov
1
,
Yu V Nelyubina
2
,
A N Kravchenko
1
,
N N Makhova
1
Publication type: Journal Article
Publication date: 2009-12-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
Abstractα-Ureidoalkylation of N-[2-(dimethylamino)ethyl]urea with 1,3-unsubstituted, 1,3-dialkyl-, and 1,3-dimethyl-4,5-diphenyl-4,5-dihydroxyimidazolidin-2-ones(thiones) was systematically studied. Hitherto unknown N-[2-(dimethylamino)ethyl]glycolurils and their hydrochlorides were synthesized. The yields of the target glycoluril hydrochlorides decreased on going from 1,3-H2- to 1,3-dialkyl-4,5-dihydroxyimidazolidin-2-ones and increased with the introduction of phenyl groups at the positions 4 and 5 of the starting 4,5-dihydroxyimidazolidin-2-one. X-ray diffraction study showed that 2-[2-(dimethylamino)ethyl]glycoluril crystallizes in the form of a conglomerate.
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Gazieva G. A. et al. 4,5-dihydroxyimidazolidin-2-ones in an α-ureidoalkylation reaction of N-(carboxyalkyl)-, N-(hydroxyalkyl)-, and N-(aminoalkyl)ureas 3. * α-Ureidoalkylation of N-[2-(dimethylamino)ethyl]urea // Russian Chemical Bulletin. 2009. Vol. 58. No. 12. pp. 2488-2493.
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Gazieva G. A., Lozhkin P. V., Baranov V., Nelyubina Yu. V., Kravchenko A. N., Makhova N. N. 4,5-dihydroxyimidazolidin-2-ones in an α-ureidoalkylation reaction of N-(carboxyalkyl)-, N-(hydroxyalkyl)-, and N-(aminoalkyl)ureas 3. * α-Ureidoalkylation of N-[2-(dimethylamino)ethyl]urea // Russian Chemical Bulletin. 2009. Vol. 58. No. 12. pp. 2488-2493.
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TY - JOUR
DO - 10.1007/s11172-009-0348-0
UR - http://link.springer.com/10.1007/s11172-009-0348-0
TI - 4,5-dihydroxyimidazolidin-2-ones in an α-ureidoalkylation reaction of N-(carboxyalkyl)-, N-(hydroxyalkyl)-, and N-(aminoalkyl)ureas 3. * α-Ureidoalkylation of N-[2-(dimethylamino)ethyl]urea
T2 - Russian Chemical Bulletin
AU - Gazieva, G A
AU - Lozhkin, P V
AU - Baranov, V.V.
AU - Nelyubina, Yu V
AU - Kravchenko, A N
AU - Makhova, N N
PY - 2009
DA - 2009/12/01
PB - Springer Nature
SP - 2488-2493
IS - 12
VL - 58
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2009_Gazieva,
author = {G A Gazieva and P V Lozhkin and V.V. Baranov and Yu V Nelyubina and A N Kravchenko and N N Makhova},
title = {4,5-dihydroxyimidazolidin-2-ones in an α-ureidoalkylation reaction of N-(carboxyalkyl)-, N-(hydroxyalkyl)-, and N-(aminoalkyl)ureas 3. * α-Ureidoalkylation of N-[2-(dimethylamino)ethyl]urea},
journal = {Russian Chemical Bulletin},
year = {2009},
volume = {58},
publisher = {Springer Nature},
month = {dec},
url = {http://link.springer.com/10.1007/s11172-009-0348-0},
number = {12},
pages = {2488--2493},
doi = {10.1007/s11172-009-0348-0}
}
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MLA
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Gazieva, G. A., et al. “4,5-dihydroxyimidazolidin-2-ones in an α-ureidoalkylation reaction of N-(carboxyalkyl)-, N-(hydroxyalkyl)-, and N-(aminoalkyl)ureas 3. * α-Ureidoalkylation of N-[2-(dimethylamino)ethyl]urea.” Russian Chemical Bulletin, vol. 58, no. 12, Dec. 2009, pp. 2488-2493. http://link.springer.com/10.1007/s11172-009-0348-0.