Influence of the steric properties of pyridine ligands on the structure of complexes containing the {LnCd2(bzo)7} fragment
M. A. Shmelev
1
,
Yu K Voronina
1
,
N. V. Gogoleva
1
,
A. A. Sidorov
1
,
M. A. Kiskin
1
,
F.M. Dolgushin
2
,
Yu V Nelyubina
2
,
G.G. Aleksandrov
1
,
E. A. Varaksina
2, 3
,
I V Taydakov
2, 3, 4
,
Publication type: Journal Article
Publication date: 2020-08-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The reaction of Cd(NO3)2 · 4H2O and Eu(NO3)3 · 6H2O or Tb(NO3)3 · 6H2O with potassium 3,5-di-tert-butylbenzoate (Kbzo) and N-donor ligands (1,10-phenanthroline (phen), 2,4-lutidine (2,4-lut), 3,4-lutidine (3,4-lut), phenanthridine (phtd), 2,3-cyclododecenopyridine (cdpy), acridine (acr)) afforded heterometallic LnCd2 complexes: [EuCd2(bzo)7(EtOH)2(phen)] (2), [LnCd2(bzo)7(2,4-lut)4] (Ln = Eu (3), Tb (4)), [EuCd2(bzo)7(H2O)2(2,4-lut)2] · MeCN (5), [EuCd2(NO3)(bzo)6(EtOH)2(2,4-lut)2] (6), [EuCd2(bzo)7(H2O)(EtOH)(3,4-lut)2] · 5EtOH (7), 3[EuCd2(bzo)7(H2O)2(phtd)2] · 4phtd (8), [EuCd2(bzo)7(EtOH)3(cdpy)] (9), 2[EuCd2-(bzo)2(EtOH)4] · acr (10). The structures of complexes 2, 3, and 5–10 were determined by single-crystal X-ray diffraction. The isostructurality of complexes 3 and 4 was confirmed by powder X-ray diffraction. The structure of the trinuclear {Ln2Cd} metal core is stable and independent of the type of peripheral ligands coordinated to cadmium atoms. Photoluminescent properties of compounds 3 and 4 were studied.
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Shmelev M. A. et al. Influence of the steric properties of pyridine ligands on the structure of complexes containing the {LnCd2(bzo)7} fragment // Russian Chemical Bulletin. 2020. Vol. 69. No. 8. pp. 1544-1560.
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Shmelev M. A., Voronina Yu. K., Gogoleva N. V., Sidorov A. A., Kiskin M. A., Dolgushin F., Nelyubina Yu. V., Aleksandrov G., Varaksina E. A., Taydakov I. V., Eremenko I. L. Influence of the steric properties of pyridine ligands on the structure of complexes containing the {LnCd2(bzo)7} fragment // Russian Chemical Bulletin. 2020. Vol. 69. No. 8. pp. 1544-1560.
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TY - JOUR
DO - 10.1007/s11172-020-2934-0
UR - https://doi.org/10.1007/s11172-020-2934-0
TI - Influence of the steric properties of pyridine ligands on the structure of complexes containing the {LnCd2(bzo)7} fragment
T2 - Russian Chemical Bulletin
AU - Shmelev, M. A.
AU - Voronina, Yu K
AU - Gogoleva, N. V.
AU - Sidorov, A. A.
AU - Kiskin, M. A.
AU - Dolgushin, F.M.
AU - Nelyubina, Yu V
AU - Aleksandrov, G.G.
AU - Varaksina, E. A.
AU - Taydakov, I V
AU - Eremenko, I. L.
PY - 2020
DA - 2020/08/01
PB - Springer Nature
SP - 1544-1560
IS - 8
VL - 69
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{2020_Shmelev,
author = {M. A. Shmelev and Yu K Voronina and N. V. Gogoleva and A. A. Sidorov and M. A. Kiskin and F.M. Dolgushin and Yu V Nelyubina and G.G. Aleksandrov and E. A. Varaksina and I V Taydakov and I. L. Eremenko},
title = {Influence of the steric properties of pyridine ligands on the structure of complexes containing the {LnCd2(bzo)7} fragment},
journal = {Russian Chemical Bulletin},
year = {2020},
volume = {69},
publisher = {Springer Nature},
month = {aug},
url = {https://doi.org/10.1007/s11172-020-2934-0},
number = {8},
pages = {1544--1560},
doi = {10.1007/s11172-020-2934-0}
}
Cite this
MLA
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Shmelev, M. A., et al. “Influence of the steric properties of pyridine ligands on the structure of complexes containing the {LnCd2(bzo)7} fragment.” Russian Chemical Bulletin, vol. 69, no. 8, Aug. 2020, pp. 1544-1560. https://doi.org/10.1007/s11172-020-2934-0.