Ceramics International, volume 48, issue 12, pages 17703-17713

Properties of ZrO2 and Ag–ZrO2 nanopowders prepared by pulsed electron beam evaporation

Sokovnin S.Yu 1, 2
Ilves V G 1
Roupcova P 3, 4
Zuev Mikhail B. 2, 5
Uimin M A 2, 6
Ulitko Maria 2
Svetlova O A 1, 2
3
 
Institute of Physics of Materials, Czech Academy of Science, Zizkova 22, 616 62, Brno, Czech Republic
4
 
CEITEC—Central European Institute of Technology, Brno University of Technology, Purkyňova 123, 612 00, Brno, Czech Republic
5
 
Institute of Solid State Chemistry, U B RAS, st. Pervomaiskaya 91, 620002, Yekaterinburg, Russia
Publication typeJournal Article
Publication date2022-06-01
Quartile SCImago
Q1
Quartile WOS
Q1
Impact factor5.2
ISSN02728842
Materials Chemistry
Surfaces, Coatings and Films
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Process Chemistry and Technology
Abstract
ZrO 2 and Ag doped ZrO 2 powders were prepared from mixtures of ZrO 2 and AgNO 3 commercial powders (99:1 and 95:5 wt %) by pulsed electron beam evaporation (PEBE) in vacuum. Samples were characterized by X-ray diffraction (XRD), transmission electron microscopy (TEM), textural and magnetic analysis, photocatalytic test, photoluminescence spectroscopy (PL) and cell cytology (Vero and Hela). XRD analysis confirmed the presence of monoclinic ZrO 2 phase and cubic Ag phase in the final product. НRTEM pictures showed a large range of particle sizes approximately from 10 to 500 nm; the spherical silver nanoparticles (NPles) (10 nm) were observed on the ZrO 2 particle surfaces. Ferromagnetic contribution in pure ZrO 2 powder was 0,002 emu/g, and in Ag doped ZrO 2 powders it reached 0,016 emu/g. It was found that Ag doped ZrO 2 powders showed increased photocatalytic activity in methyl orange (MO) compared with pure ZrO 2 NPles. The produced powders can be used to kill Hela cancer cells, as low (<0.1 wt) Ag photocatalysts and in other applications.

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Sokovnin S. et al. Properties of ZrO2 and Ag–ZrO2 nanopowders prepared by pulsed electron beam evaporation // Ceramics International. 2022. Vol. 48. No. 12. pp. 17703-17713.
GOST all authors (up to 50) Copy
Sokovnin S., Pizúrová N., Ilves V. G., Roupcova P., Zuev M. B., Uimin M. A., Ulitko M., Svetlova O. A. Properties of ZrO2 and Ag–ZrO2 nanopowders prepared by pulsed electron beam evaporation // Ceramics International. 2022. Vol. 48. No. 12. pp. 17703-17713.
RIS |
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TY - JOUR
DO - 10.1016/j.ceramint.2022.03.040
UR - https://doi.org/10.1016%2Fj.ceramint.2022.03.040
TI - Properties of ZrO2 and Ag–ZrO2 nanopowders prepared by pulsed electron beam evaporation
T2 - Ceramics International
AU - Sokovnin, S.Yu
AU - Pizúrová, N.
AU - Ilves, V G
AU - Roupcova, P
AU - Zuev, Mikhail B.
AU - Uimin, M A
AU - Ulitko, Maria
AU - Svetlova, O A
PY - 2022
DA - 2022/06/01 00:00:00
PB - Elsevier
SP - 17703-17713
IS - 12
VL - 48
SN - 0272-8842
ER -
BibTex |
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BibTex Copy
@article{2022_Sokovnin,
author = {S.Yu Sokovnin and N. Pizúrová and V G Ilves and P Roupcova and Mikhail B. Zuev and M A Uimin and Maria Ulitko and O A Svetlova},
title = {Properties of ZrO2 and Ag–ZrO2 nanopowders prepared by pulsed electron beam evaporation},
journal = {Ceramics International},
year = {2022},
volume = {48},
publisher = {Elsevier},
month = {jun},
url = {https://doi.org/10.1016%2Fj.ceramint.2022.03.040},
number = {12},
pages = {17703--17713},
doi = {10.1016/j.ceramint.2022.03.040}
}
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Sokovnin, S.Yu, et al. “Properties of ZrO2 and Ag–ZrO2 nanopowders prepared by pulsed electron beam evaporation.” Ceramics International, vol. 48, no. 12, Jun. 2022, pp. 17703-17713. https://doi.org/10.1016%2Fj.ceramint.2022.03.040.
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