NMR approach for the identification of dinuclear and mononuclear complexes: The first detection of [Pd(SPh)2 (PPh3 )2 ] and [Pd2 (SPh)4 (PPh3 )2 ] - The intermediate complexes in the catalytic carbon-sulfur bond formation reaction
Publication type: Journal Article
Publication date: 2011-01-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract In the present study we have analyzed the nature of palladium complexes in the catalytic system for selective carbon–sulfur bond formation via the addition of S–S and S–H bonds to alkynes. For the first time the mononuclear and dinuclear palladium complexes were clearly detected by DOSY NMR under the catalytic conditions. It was demonstrated that the concentration of these palladium complexes strongly depends on the amount of phosphine ligand available under reaction conditions.
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Metrics
27
Total citations:
27
Citations from 2024:
2
(7%)
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GOST
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Ananikov V. P. et al. NMR approach for the identification of dinuclear and mononuclear complexes: The first detection of [Pd(SPh)2(PPh3)2] and [Pd2(SPh)4(PPh3)2] - The intermediate complexes in the catalytic carbon-sulfur bond formation reaction // Journal of Organometallic Chemistry. 2011. Vol. 696. No. 1. pp. 400-405.
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Ananikov V. P., Kachala V. V., S. Zalesskiy S., Beletskaya I. P. NMR approach for the identification of dinuclear and mononuclear complexes: The first detection of [Pd(SPh)2(PPh3)2] and [Pd2(SPh)4(PPh3)2] - The intermediate complexes in the catalytic carbon-sulfur bond formation reaction // Journal of Organometallic Chemistry. 2011. Vol. 696. No. 1. pp. 400-405.
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RIS
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TY - JOUR
DO - 10.1016/j.jorganchem.2010.10.012
UR - https://doi.org/10.1016/j.jorganchem.2010.10.012
TI - NMR approach for the identification of dinuclear and mononuclear complexes: The first detection of [Pd(SPh)2(PPh3)2] and [Pd2(SPh)4(PPh3)2] - The intermediate complexes in the catalytic carbon-sulfur bond formation reaction
T2 - Journal of Organometallic Chemistry
AU - Ananikov, Valentine P.
AU - Kachala, Vadim V.
AU - S. Zalesskiy, Sergey
AU - Beletskaya, Irina P.
PY - 2011
DA - 2011/01/01
PB - Elsevier
SP - 400-405
IS - 1
VL - 696
SN - 0022-328X
SN - 1872-8561
ER -
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BibTex (up to 50 authors)
Copy
@article{2011_Ananikov,
author = {Valentine P. Ananikov and Vadim V. Kachala and Sergey S. Zalesskiy and Irina P. Beletskaya},
title = {NMR approach for the identification of dinuclear and mononuclear complexes: The first detection of [Pd(SPh)2(PPh3)2] and [Pd2(SPh)4(PPh3)2] - The intermediate complexes in the catalytic carbon-sulfur bond formation reaction},
journal = {Journal of Organometallic Chemistry},
year = {2011},
volume = {696},
publisher = {Elsevier},
month = {jan},
url = {https://doi.org/10.1016/j.jorganchem.2010.10.012},
number = {1},
pages = {400--405},
doi = {10.1016/j.jorganchem.2010.10.012}
}
Cite this
MLA
Copy
Ananikov, Valentine P., et al. “NMR approach for the identification of dinuclear and mononuclear complexes: The first detection of [Pd(SPh)2(PPh3)2] and [Pd2(SPh)4(PPh3)2] - The intermediate complexes in the catalytic carbon-sulfur bond formation reaction.” Journal of Organometallic Chemistry, vol. 696, no. 1, Jan. 2011, pp. 400-405. https://doi.org/10.1016/j.jorganchem.2010.10.012.
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