Calcium-based coordination polymers from a solvothermal synthesis of HKUST-1 in 3D printed autoclaves
Тип публикации: Journal Article
Дата публикации: 2022-01-01
scimago Q3
wos Q3
БС1
SJR: 0.305
CiteScore: 3.0
Impact factor: 1.7
ISSN: 09599436, 1364551X
General Chemistry
Краткое описание
A mixed-metal 1D coordination polymer [CaCu(HBTC) 2 (H2O) 8 ] n (where H 3 BTC – benzene-1,3,5-tric arboxylic acid) was obtained in a solvothermal synthesis of a well-known copper-containing metal–organic framework [Cu 3 (BTC) 2 (H 2 O) 3 ] n (HKUST-1) in autoclaves 3D-printed from commercial polypropylene. This material was a source of calcium ions, apparently, leaking from a colorant (calcium carbonate) promoted by glacial acetic acid as a modulator used to produce large single crystals of HKUST-1. This finding was confirmed by elemental analysis and a model experiment that resulted in a new calcium-based 1D coordination polymer [Ca(H 2 BTC) 2 (H 2 O) 5 ] n under the same solvothermal conditions with no copper or calcium salts put into a 3D-printed autoclave.
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Denisov G. L. et al. Calcium-based coordination polymers from a solvothermal synthesis of HKUST-1 in 3D printed autoclaves // Mendeleev Communications. 2022. Vol. 32. No. 1. pp. 105-108.
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Primakov P. V., Lependina O. L., Denisov G. S., Novikov V. V., Korlyukov A., Nelyubina Y. V. Calcium-based coordination polymers from a solvothermal synthesis of HKUST-1 in 3D printed autoclaves // Mendeleev Communications. 2022. Vol. 32. No. 1. pp. 105-108.
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TY - JOUR
DO - 10.1016/j.mencom.2022.01.034
UR - https://doi.org/10.1016/j.mencom.2022.01.034
TI - Calcium-based coordination polymers from a solvothermal synthesis of HKUST-1 in 3D printed autoclaves
T2 - Mendeleev Communications
AU - Primakov, Petr V
AU - Lependina, Olga L
AU - Denisov, Gleb S.
AU - Novikov, Valentin V
AU - Korlyukov, Alexander
AU - Nelyubina, Yulia V.
PY - 2022
DA - 2022/01/01
PB - OOO Zhurnal "Mendeleevskie Soobshcheniya"
SP - 105-108
IS - 1
VL - 32
SN - 0959-9436
SN - 1364-551X
ER -
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@article{2022_Denisov,
author = {Petr V Primakov and Olga L Lependina and Gleb S. Denisov and Valentin V Novikov and Alexander Korlyukov and Yulia V. Nelyubina},
title = {Calcium-based coordination polymers from a solvothermal synthesis of HKUST-1 in 3D printed autoclaves},
journal = {Mendeleev Communications},
year = {2022},
volume = {32},
publisher = {OOO Zhurnal "Mendeleevskie Soobshcheniya"},
month = {jan},
url = {https://doi.org/10.1016/j.mencom.2022.01.034},
number = {1},
pages = {105--108},
doi = {10.1016/j.mencom.2022.01.034}
}
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MLA
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Denisov, Gleb L., et al. “Calcium-based coordination polymers from a solvothermal synthesis of HKUST-1 in 3D printed autoclaves.” Mendeleev Communications, vol. 32, no. 1, Jan. 2022, pp. 105-108. https://doi.org/10.1016/j.mencom.2022.01.034.
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