Neutral tetranuclear Cu(II) complex of 2,6-di(5-trifluoromethylpyrazol-3-yl)pyridine: Synthesis, characterization and its transformation with selected aza-ligands
Ekaterina F. Zhilina
1
,
Dmitrii L Chizhov
1
,
Yuri N Shvachko
2
,
Grigory G. Aleksandrov
3
,
Alexandr V Korolev
2
,
Valeriy N Charushin
1
,
A.V Sidorov
3
,
Matvey Fedin
4
,
Publication type: Journal Article
Publication date: 2013-04-01
scimago Q3
wos Q2
SJR: 0.396
CiteScore: 4.9
Impact factor: 2.6
ISSN: 02775387, 18733719
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Abstract New tetranuclear Cu(II) complex [Cu4(L)4]·MeCN (1) with 2,6-di(5-trifluoromethyl-1H-pyrazol-3-yl)pyridine (H2L) was synthesized. It has been shown that treatment of 1 with selected aza-ligands (pyridine, 2,2′- and 4,4′-bipyridyl, 2,3,5,6-tetra-(pyridine-2-yl)pyrazine, 2,2′;6′,2″-terpyridine and 1,4-diazabicyclo[2.2.2]octane) leads to formation of other Cu(II) complexes with different nuclearity: [Cu(L)py2] (2), [Cu(L)(2,2′-bpy)] (3), [Cu(L)2(tppz)]·THF (5), [Cu(L)tpy]·C6H5CN (4), {[Cu2(L)2(4,4′-bpy)2]·(C6H5CH3)·MeCN}n (6) and {[Cu(L)DABCO]·2MeCN}n (7). Obtained compounds were characterized by IR spectroscopy, X-ray crystallography data, EPR and SQUID magnetic measurements.
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Zhilina E. F. et al. Neutral tetranuclear Cu(II) complex of 2,6-di(5-trifluoromethylpyrazol-3-yl)pyridine: Synthesis, characterization and its transformation with selected aza-ligands // Polyhedron. 2013. Vol. 53. pp. 122-131.
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Zhilina E. F., Chizhov D. L., Slepukhin P. A., Shvachko Y. N., Aleksandrov G. G., Korolev A. V., Charushin V. N., Sidorov A., Kiskin M. A., Fedin M., Starichenko D., Eremenko I. L. Neutral tetranuclear Cu(II) complex of 2,6-di(5-trifluoromethylpyrazol-3-yl)pyridine: Synthesis, characterization and its transformation with selected aza-ligands // Polyhedron. 2013. Vol. 53. pp. 122-131.
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TY - JOUR
DO - 10.1016/j.poly.2013.01.021
UR - https://doi.org/10.1016/j.poly.2013.01.021
TI - Neutral tetranuclear Cu(II) complex of 2,6-di(5-trifluoromethylpyrazol-3-yl)pyridine: Synthesis, characterization and its transformation with selected aza-ligands
T2 - Polyhedron
AU - Zhilina, Ekaterina F.
AU - Chizhov, Dmitrii L
AU - Slepukhin, Pavel A.
AU - Shvachko, Yuri N
AU - Aleksandrov, Grigory G.
AU - Korolev, Alexandr V
AU - Charushin, Valeriy N
AU - Sidorov, A.V
AU - Kiskin, Mikhail A.
AU - Fedin, Matvey
AU - Starichenko, Denis
AU - Eremenko, Igor L.
PY - 2013
DA - 2013/04/01
PB - Elsevier
SP - 122-131
VL - 53
SN - 0277-5387
SN - 1873-3719
ER -
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@article{2013_Zhilina,
author = {Ekaterina F. Zhilina and Dmitrii L Chizhov and Pavel A. Slepukhin and Yuri N Shvachko and Grigory G. Aleksandrov and Alexandr V Korolev and Valeriy N Charushin and A.V Sidorov and Mikhail A. Kiskin and Matvey Fedin and Denis Starichenko and Igor L. Eremenko},
title = {Neutral tetranuclear Cu(II) complex of 2,6-di(5-trifluoromethylpyrazol-3-yl)pyridine: Synthesis, characterization and its transformation with selected aza-ligands},
journal = {Polyhedron},
year = {2013},
volume = {53},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/j.poly.2013.01.021},
pages = {122--131},
doi = {10.1016/j.poly.2013.01.021}
}